C₁₃H₁₂S

Base Information

Chemical Name:C₁₃H₁₂S
CAS No.:1334512-05-8
Molecular Formula:C₁₃H₁₂S
Molecular Weight:200.304
Hs Code.:

Synonyms:C₁₃H₁₂S

Suppliers and Price of C₁₃H₁₂S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₃H₁₂S

Chemical Property:

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Technology Process of C₁₃H₁₂S

There total 3 articles about C₁₃H₁₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 905966-46-3
5,5-dimethyl-2-(thiophen-3-yl)-1,3,2-dioxaborinane

: diethyl 3-phenylprop-2-enyl phosphate

: 133039-41-5
3-cinnamylthiophene

: 1334512-05-8
C₁₃H₁₂S

Guidance literature:: With C₂₆H₂₂N₂O*F₆P^(1-)*H⁽¹⁺⁾; sodium methylate; copper(l) chloride; In tetrahydrofuran; at 30 ℃; for 16h; optical yield given as %ee; enantioselective reaction;
DOI:10.1002/anie.201103581

Reference yield:

: 1334511-96-4
diethyl (E)-3-(3-thienyl)-2-propenyl phosphate

: 5123-13-7
5,5-dimethyl-2-phenyl-1,3,2-dioxaborinane

: 1334512-09-2
C₁₃H₁₂S

: 1334512-05-8
C₁₃H₁₂S

Guidance literature:: With C₂₆H₂₂N₂O*F₆P^(1-)*H⁽¹⁺⁾; sodium methylate; copper(l) chloride; In tetrahydrofuran; at 30 ℃; for 16h; optical yield given as %ee; enantioselective reaction;
DOI:10.1002/anie.201103581

Reference yield:

: 50266-60-9
(E)-3-thiophen-3-yl-acrylic acid ethyl ester

: 1334512-09-2
C₁₃H₁₂S

: 1334512-05-8
C₁₃H₁₂S

Guidance literature:: Multi-step reaction with 3 steps

1: diisobutylaluminium hydride / hexane; toluene / 4 h / -78 - 20 °C

2: dmap; triethylamine / dichloromethane / 9 h / 0 - 20 °C

3: C₂₆H₂₂N₂O*F₆P^(1-)*H⁽¹⁺⁾; sodium methylate; copper(l) chloride / tetrahydrofuran / 16 h / 30 °C

With dmap; C₂₆H₂₂N₂O*F₆P^(1-)*H⁽¹⁺⁾; sodium methylate; diisobutylaluminium hydride; triethylamine; copper(l) chloride; In tetrahydrofuran; hexane; dichloromethane; toluene;
DOI:10.1002/anie.201103581