trifluoromethyl-sulfenyl acetate

Base Information

• Chemical Name: trifluoromethyl-sulfenyl acetate
• CAS No.: 42530-92-7
• Molecular Formula: C₃H₃F₃O₂S
• Molecular Weight: 160.117
• Mol file: 42530-92-7.mol

Synonyms:trifluoromethyl-sulfenyl acetate

Chemical Property of trifluoromethyl-sulfenyl acetate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of trifluoromethyl-sulfenyl acetate

There total 1 articles about trifluoromethyl-sulfenyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

Trifluoromethylsulfenyl chloride (421-17-0) + sodium acetate (127-09-3) → Bis(trifluoromethyl)disulfid (372-64-5) + Trifluoro-methanethiosulfonic acid S-trifluoromethyl ester (358-15-6) + trifluoromethyl-sulfenyl acetate (42530-92-7) + acetic anhydride (108-24-7)

Guidance literature:

at 0 ℃; for 12h;

DOI:10.1016/S0022-1139(00)82329-5

Reference yield: 73.0%

trifluoromethyl-sulfenyl acetate (42530-92-7) + 1,3,5-trimethyl-benzene (108-67-8) → 1,3,5-trimethyl-2-[(trifluoromethyl)sulfanyl]benzene (103548-34-1)

Guidance literature:

at 0 - 20 ℃; for 1h;

DOI:10.1016/S0022-1139(00)82329-5

Reference yield: 55.0%

trifluoromethyl-sulfenyl acetate (42530-92-7) + cyclohexene (110-83-8) → Acetic acid (1S,2S)-2-trifluoromethylsulfanyl-cyclohexyl ester

Guidance literature:

at 20 ℃; for 5h;

DOI:10.1016/S0022-1139(00)82329-5

upstream raw materials:

Trifluoromethylsulfenyl chloride

sodium acetate

Downstream raw materials:

4-trifluoromethylthiotoluene

1-methyl-2-[(trifluoromethyl)thio]benzene

1,3,5-trimethyl-2-[(trifluoromethyl)sulfanyl]benzene