methyl 10-[2-methoxy-4-(3-trifluoromethyl-3H-diazirin-3-yl)phenyl]-10-oxodecanoate

Base Information

Chemical Name:methyl 10-[2-methoxy-4-(3-trifluoromethyl-3H-diazirin-3-yl)phenyl]-10-oxodecanoate
CAS No.:523227-16-9
Molecular Formula:C₂₀H₂₅F₃N₂O₄
Molecular Weight:414.425
Hs Code.:

Synonyms:methyl 10-[2-methoxy-4-(3-trifluoromethyl-3H-diazirin-3-yl)phenyl]-10-oxodecanoate

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Chemical Property of methyl 10-[2-methoxy-4-(3-trifluoromethyl-3H-diazirin-3-yl)phenyl]-10-oxodecanoate

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Technology Process of methyl 10-[2-methoxy-4-(3-trifluoromethyl-3H-diazirin-3-yl)phenyl]-10-oxodecanoate

There total 1 articles about methyl 10-[2-methoxy-4-(3-trifluoromethyl-3H-diazirin-3-yl)phenyl]-10-oxodecanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 14065-32-8
methyl 10-chloro-10-oxodecanoate

: 205485-24-1
3-(3-methoxyphenyl)-3-(trifluoromethyl)-3H-diazirine

: 523227-16-9
methyl 10-[2-methoxy-4-(3-trifluoromethyl-3H-diazirin-3-yl)phenyl]-10-oxodecanoate

Guidance literature:: With titanium chloride; at 20 ℃; for 8h;
DOI:10.3987/COM-02-S16

Reference yield: 95.0%

: 523227-16-9
methyl 10-[2-methoxy-4-(3-trifluoromethyl-3H-diazirin-3-yl)phenyl]-10-oxodecanoate

: 523227-17-0
methyl 10-[2-methoxy-4-(3-trifluoromethyl-3H-diazirin-3-yl)phenyl]decanoate

Guidance literature:: With triethylsilane; trifluoroacetic acid; at 20 ℃; for 0.166667h;
DOI:10.3987/COM-02-S16

Reference yield:

: 523227-16-9
methyl 10-[2-methoxy-4-(3-trifluoromethyl-3H-diazirin-3-yl)phenyl]-10-oxodecanoate

: 10-[2-methoxy-4-(3-trifluoromethyl-3H-diazirin-3-yl)phenyl]decanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / trifluoroacetic acid; triethylsilane / 0.17 h / 20 °C

2: 89 percent / sodium hydroxide / methanol / 2 h / 20 °C

With triethylsilane; sodium hydroxide; trifluoroacetic acid; In methanol;
DOI:10.3987/COM-02-S16