methyl 10-[2-methoxy-4-(3-trifluoromethyl-3H-diazirin-3-yl)phenyl]decanoate

Base Information

• Chemical Name: methyl 10-[2-methoxy-4-(3-trifluoromethyl-3H-diazirin-3-yl)phenyl]decanoate
• CAS No.: 523227-17-0
• Molecular Formula: C₂₀H₂₇F₃N₂O₃
• Molecular Weight: 400.441

Synonyms:methyl 10-[2-methoxy-4-(3-trifluoromethyl-3H-diazirin-3-yl)phenyl]decanoate

Chemical Property of methyl 10-[2-methoxy-4-(3-trifluoromethyl-3H-diazirin-3-yl)phenyl]decanoate

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Technology Process of methyl 10-[2-methoxy-4-(3-trifluoromethyl-3H-diazirin-3-yl)phenyl]decanoate

There total 3 articles about methyl 10-[2-methoxy-4-(3-trifluoromethyl-3H-diazirin-3-yl)phenyl]decanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

methyl 10-[2-methoxy-4-(3-trifluoromethyl-3H-diazirin-3-yl)phenyl]-10-oxodecanoate (523227-16-9) → methyl 10-[2-methoxy-4-(3-trifluoromethyl-3H-diazirin-3-yl)phenyl]decanoate (523227-17-0)

Guidance literature:

With triethylsilane; trifluoroacetic acid; at 20 ℃; for 0.166667h;

DOI:10.3987/COM-02-S16

Reference yield:

methyl 10-chloro-10-oxodecanoate (14065-32-8) → methyl 10-[2-methoxy-4-(3-trifluoromethyl-3H-diazirin-3-yl)phenyl]decanoate (523227-17-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 43 percent / titanium chloride / 8 h / 20 °C

2: 95 percent / trifluoroacetic acid; triethylsilane / 0.17 h / 20 °C

With triethylsilane; titanium chloride; trifluoroacetic acid; 1: Friedel-Crafts acylation;

DOI:10.3987/COM-02-S16

Reference yield:

3-(3-methoxyphenyl)-3-(trifluoromethyl)-3H-diazirine (205485-24-1) → methyl 10-[2-methoxy-4-(3-trifluoromethyl-3H-diazirin-3-yl)phenyl]decanoate (523227-17-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 43 percent / titanium chloride / 8 h / 20 °C

2: 95 percent / trifluoroacetic acid; triethylsilane / 0.17 h / 20 °C

With triethylsilane; titanium chloride; trifluoroacetic acid; 1: Friedel-Crafts acylation;

DOI:10.3987/COM-02-S16

upstream raw materials:

methyl 10-[2-methoxy-4-(3-trifluoromethyl-3H-diazirin-3-yl)phenyl]-10-oxodecanoate

methyl 10-chloro-10-oxodecanoate

3-(3-methoxyphenyl)-3-(trifluoromethyl)-3H-diazirine

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