o-nitrophenylthioiminocyclopentane

Base Information

• Chemical Name: o-nitrophenylthioiminocyclopentane
• CAS No.: 127901-86-4
• Molecular Formula: C₁₁H₁₂N₂O₂S
• Molecular Weight: 236.294

Synonyms:o-nitrophenylthioiminocyclopentane

Chemical Property of o-nitrophenylthioiminocyclopentane

Chemical Property:

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Technology Process of o-nitrophenylthioiminocyclopentane

There total 1 articles about o-nitrophenylthioiminocyclopentane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-nitrobenzenesulfenamide (7257-59-2) + cyclopentanone (120-92-3) → o-nitrophenylthioiminocyclopentane (127901-86-4)

Guidance literature:

With benzenesulfonic acid; In benzene; Heating;

DOI:10.1248/cpb.37.3393

Reference yield: 57.5%

methanol (67-56-1) + o-nitrophenylthioiminocyclopentane (127901-86-4) → methyl-2-nitrobenzenesulphinate (30388-71-7) + cyclopentanone (120-92-3)

Guidance literature:

With water; sodium perchlorate; Ambient temperature; electrolysis;

DOI:10.1248/cpb.37.3393

Reference yield: 11.3%

o-nitrophenylthioiminocyclopentane (127901-86-4) → bis(2-nitrophenyl)disulfide (1155-00-6) + N,2,2-tris(o-nitrophenylthio)iminocyclopentane (127901-91-1) + cyclopentanone (120-92-3)

Guidance literature:

sodium perchlorate; In acetonitrile; Ambient temperature; electrolysis;

DOI:10.1248/cpb.37.3393

upstream raw materials:

2-nitrobenzenesulfenamide

cyclopentanone

Downstream raw materials:

methyl-2-nitrobenzenesulphinate

cyclopentanone

bis(2-nitrophenyl)disulfide

N,2,2-tris(o-nitrophenylthio)iminocyclopentane

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