3-(N-tert-butyldimethylsiloxy-N-tert-butylamino)-5-tert-butylbenzophenone

Base Information

Chemical Name:3-(N-tert-butyldimethylsiloxy-N-tert-butylamino)-5-tert-butylbenzophenone
CAS No.:179061-64-4
Molecular Formula:C₂₇H₄₁NO₂Si
Molecular Weight:439.714
Hs Code.:

Synonyms:3-(N-tert-butyldimethylsiloxy-N-tert-butylamino)-5-tert-butylbenzophenone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(N-tert-butyldimethylsiloxy-N-tert-butylamino)-5-tert-butylbenzophenone

Chemical Property:

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Technology Process of 3-(N-tert-butyldimethylsiloxy-N-tert-butylamino)-5-tert-butylbenzophenone

There total 4 articles about 3-(N-tert-butyldimethylsiloxy-N-tert-butylamino)-5-tert-butylbenzophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 179061-63-3
C₂₇H₄₃NO₂Si

: 179061-64-4
3-(N-tert-butyldimethylsiloxy-N-tert-butylamino)-5-tert-butylbenzophenone

Guidance literature:: With dipyridinium dichromate; In dichloromethane;
DOI:10.1039/cc9960001131

Reference yield:

: 133817-83-1
N-(3-bromo-5-tert-butylphenyl)-N-(tert-butyldimethylsiloxy)-N-tert-butylamine

: 179061-64-4
3-(N-tert-butyldimethylsiloxy-N-tert-butylamino)-5-tert-butylbenzophenone

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) n-BuLi / 1.) THF, hexane, -78 deg C, 45 min, 2.) -78 deg C to 25 deg C

2: 53 percent / pyridinium dichromate / CH₂Cl₂ / 3 h

With dipyridinium dichromate; n-butyllithium; In dichloromethane;
DOI:10.1039/a801680a

Reference yield:

: 100-52-7
benzaldehyde

: 179061-64-4
3-(N-tert-butyldimethylsiloxy-N-tert-butylamino)-5-tert-butylbenzophenone

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) BuLi / 1.) THF, -78 deg C

2: 53 percent / PDC / CH₂Cl₂

With dipyridinium dichromate; n-butyllithium; In dichloromethane;
DOI:10.1039/cc9960001131