3-(N-tert-butyldimethylsiloxy-N-tert-butylamino)-5-tert-butylbenzophenone hydrazone

Base Information

Chemical Name:3-(N-tert-butyldimethylsiloxy-N-tert-butylamino)-5-tert-butylbenzophenone hydrazone
CAS No.:179061-65-5
Molecular Formula:C₂₇H₄₃N₃OSi
Molecular Weight:453.743
Hs Code.:

Synonyms:3-(N-tert-butyldimethylsiloxy-N-tert-butylamino)-5-tert-butylbenzophenone hydrazone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(N-tert-butyldimethylsiloxy-N-tert-butylamino)-5-tert-butylbenzophenone hydrazone

Chemical Property:

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Technology Process of 3-(N-tert-butyldimethylsiloxy-N-tert-butylamino)-5-tert-butylbenzophenone hydrazone

There total 4 articles about 3-(N-tert-butyldimethylsiloxy-N-tert-butylamino)-5-tert-butylbenzophenone hydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 179061-64-4
3-(N-tert-butyldimethylsiloxy-N-tert-butylamino)-5-tert-butylbenzophenone

: 179061-65-5
3-(N-tert-butyldimethylsiloxy-N-tert-butylamino)-5-tert-butylbenzophenone hydrazone

Guidance literature:: With triazene 1-nitrogen; In ethanol; Heating;
DOI:10.1039/cc9960001131

Reference yield:

: 133817-83-1
N-(3-bromo-5-tert-butylphenyl)-N-(tert-butyldimethylsiloxy)-N-tert-butylamine

: 179061-65-5
3-(N-tert-butyldimethylsiloxy-N-tert-butylamino)-5-tert-butylbenzophenone hydrazone

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) n-BuLi / 1.) THF, hexane, -78 deg C, 45 min, 2.) -78 deg C to 25 deg C

2: 53 percent / pyridinium dichromate / CH₂Cl₂ / 3 h

3: 81 percent / H₂NNH₂*H₂O / ethanol / 20 h / Heating

With dipyridinium dichromate; n-butyllithium; hydrazine hydrate; In ethanol; dichloromethane;
DOI:10.1039/a801680a

Reference yield:

: 100-52-7
benzaldehyde

: 179061-65-5
3-(N-tert-butyldimethylsiloxy-N-tert-butylamino)-5-tert-butylbenzophenone hydrazone

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) BuLi / 1.) THF, -78 deg C

2: 53 percent / PDC / CH₂Cl₂

3: 81 percent / N₄H₄*H₂O / ethanol / Heating

With dipyridinium dichromate; n-butyllithium; triazene 1-nitrogen; In ethanol; dichloromethane;
DOI:10.1039/cc9960001131