4-(3-(tert-butoxy)-3-oxopropyl)-2,6-diisopropylphenyl 7-azido-4-oxoheptanoate

Base Information

• Chemical Name: 4-(3-(tert-butoxy)-3-oxopropyl)-2,6-diisopropylphenyl 7-azido-4-oxoheptanoate
• CAS No.: 1254943-32-2
• Molecular Formula: C₂₆H₃₉N₃O₅
• Molecular Weight: 473.613

Synonyms:4-(3-(tert-butoxy)-3-oxopropyl)-2,6-diisopropylphenyl 7-azido-4-oxoheptanoate

Chemical Property of 4-(3-(tert-butoxy)-3-oxopropyl)-2,6-diisopropylphenyl 7-azido-4-oxoheptanoate

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Technology Process of 4-(3-(tert-butoxy)-3-oxopropyl)-2,6-diisopropylphenyl 7-azido-4-oxoheptanoate

There total 1 articles about 4-(3-(tert-butoxy)-3-oxopropyl)-2,6-diisopropylphenyl 7-azido-4-oxoheptanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

7-azido-4-oxoheptanoic acid (1254943-31-1) + tert-butyl 3-(4-hydroxy-3,5-diisopropylphenyl)propanoate (1254943-27-5) → 4-(3-(tert-butoxy)-3-oxopropyl)-2,6-diisopropylphenyl 7-azido-4-oxoheptanoate (1254943-32-2)

Guidance literature:

With dmap; diisopropyl-carbodiimide; In dichloromethane; for 14h;

DOI:10.1002/anie.201001767

Reference yield: 100.0%

4-(3-(tert-butoxy)-3-oxopropyl)-2,6-diisopropylphenyl 7-azido-4-oxoheptanoate (1254943-32-2) + Fmoc-N-propargylamine (127896-08-6) → 4-(3-(tert-butoxy)-3-oxopropyl)-2,6-diisopropylphenyl 7-(4-(((((9H-fluoren-9-yl)methoxy)carbonyl)amino)methyl)-1H-1,2,3-triazol-1-yl)-4-oxoheptanoate (1357309-72-8)

Guidance literature:

With copper(II) sulfate; sodium L-ascorbate; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine; In water; tert-butyl alcohol; at 20 ℃; for 16h; Inert atmosphere;

DOI:10.1016/j.bmc.2011.07.049

Reference yield: 100.0%

4-(3-(tert-butoxy)-3-oxopropyl)-2,6-diisopropylphenyl 7-azido-4-oxoheptanoate (1254943-32-2) → 3-(4-((7-azido-4-oxoheptanoyl)oxy)-3,5-diisopropylphenyl)propanoic acid (1254943-33-3)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; for 0.5h;

DOI:10.1002/anie.201001767

upstream raw materials:

7-azido-4-oxoheptanoic acid

tert-butyl 3-(4-hydroxy-3,5-diisopropylphenyl)propanoate

Downstream raw materials:

3-(4-((7-azido-4-oxoheptanoyl)oxy)-3,5-diisopropylphenyl)propanoic acid

C₄₀H₄₆N₄O₇

4-(3-((2,5-dioxopyrrolidin-1-yl)oxy)-3-oxopropyl)-2,6-di-isopropylphenyl 7-(4-(((((9H-fluoren-9-yl)methoxy)carbonyl)-amino)methyl)-1H-1,2,3-triazol-1-yl)-4-oxoheptanoate

4-(3-(tert-butoxy)-3-oxopropyl)-2,6-diisopropylphenyl 7-(4-(((((9H-fluoren-9-yl)methoxy)carbonyl)amino)methyl)-1H-1,2,3-triazol-1-yl)-4-oxoheptanoate

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