4-(3-(tert-butoxy)-3-oxopropyl)-2,6-diisopropylphenyl 7-(4-(((((9H-fluoren-9-yl)methoxy)carbonyl)amino)methyl)-1H-1,2,3-triazol-1-yl)-4-oxoheptanoate

Base Information

Chemical Name:4-(3-(tert-butoxy)-3-oxopropyl)-2,6-diisopropylphenyl 7-(4-(((((9H-fluoren-9-yl)methoxy)carbonyl)amino)methyl)-1H-1,2,3-triazol-1-yl)-4-oxoheptanoate
CAS No.:1357309-72-8
Molecular Formula:C₄₄H₅₄N₄O₇
Molecular Weight:750.935
Hs Code.:

Synonyms:4-(3-(tert-butoxy)-3-oxopropyl)-2,6-diisopropylphenyl 7-(4-(((((9H-fluoren-9-yl)methoxy)carbonyl)amino)methyl)-1H-1,2,3-triazol-1-yl)-4-oxoheptanoate

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Chemical Property of 4-(3-(tert-butoxy)-3-oxopropyl)-2,6-diisopropylphenyl 7-(4-(((((9H-fluoren-9-yl)methoxy)carbonyl)amino)methyl)-1H-1,2,3-triazol-1-yl)-4-oxoheptanoate

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Technology Process of 4-(3-(tert-butoxy)-3-oxopropyl)-2,6-diisopropylphenyl 7-(4-(((((9H-fluoren-9-yl)methoxy)carbonyl)amino)methyl)-1H-1,2,3-triazol-1-yl)-4-oxoheptanoate

There total 1 articles about 4-(3-(tert-butoxy)-3-oxopropyl)-2,6-diisopropylphenyl 7-(4-(((((9H-fluoren-9-yl)methoxy)carbonyl)amino)methyl)-1H-1,2,3-triazol-1-yl)-4-oxoheptanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1254943-32-2
4-(3-(tert-butoxy)-3-oxopropyl)-2,6-diisopropylphenyl 7-azido-4-oxoheptanoate

: 127896-08-6
Fmoc-N-propargylamine

: 1357309-72-8
4-(3-(tert-butoxy)-3-oxopropyl)-2,6-diisopropylphenyl 7-(4-(((((9H-fluoren-9-yl)methoxy)carbonyl)amino)methyl)-1H-1,2,3-triazol-1-yl)-4-oxoheptanoate

Guidance literature:: With copper(II) sulfate; sodium L-ascorbate; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine; In water; tert-butyl alcohol; at 20 ℃; for 16h; Inert atmosphere;
DOI:10.1016/j.bmc.2011.07.049

Reference yield:

: 1357309-72-8
4-(3-(tert-butoxy)-3-oxopropyl)-2,6-diisopropylphenyl 7-(4-(((((9H-fluoren-9-yl)methoxy)carbonyl)amino)methyl)-1H-1,2,3-triazol-1-yl)-4-oxoheptanoate

: 1357309-73-9
C₄₀H₄₆N₄O₇

Guidance literature:: With trifluoroacetic acid; In dichloromethane; for 1h; Inert atmosphere;
DOI:10.1016/j.bmc.2011.07.049

Reference yield:

: 1357309-72-8
4-(3-(tert-butoxy)-3-oxopropyl)-2,6-diisopropylphenyl 7-(4-(((((9H-fluoren-9-yl)methoxy)carbonyl)amino)methyl)-1H-1,2,3-triazol-1-yl)-4-oxoheptanoate

: 1357309-74-0
4-(3-((2,5-dioxopyrrolidin-1-yl)oxy)-3-oxopropyl)-2,6-di-isopropylphenyl 7-(4-(((((9H-fluoren-9-yl)methoxy)carbonyl)-amino)methyl)-1H-1,2,3-triazol-1-yl)-4-oxoheptanoate

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / dichloromethane / 1 h / Inert atmosphere

2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 40 h / Inert atmosphere

With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid; In dichloromethane;
DOI:10.1016/j.bmc.2011.07.049