1-benzyl-2,6-dioxo-1,2,3,6-tetrahydropyridine-4-carboxylic acid ethyl ester

Base Information

Chemical Name:1-benzyl-2,6-dioxo-1,2,3,6-tetrahydropyridine-4-carboxylic acid ethyl ester
CAS No.:503545-00-4
Molecular Formula:C₁₅H₁₅NO₄
Molecular Weight:273.288
Hs Code.:

Synonyms:1-benzyl-2,6-dioxo-1,2,3,6-tetrahydropyridine-4-carboxylic acid ethyl ester

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Chemical Property of 1-benzyl-2,6-dioxo-1,2,3,6-tetrahydropyridine-4-carboxylic acid ethyl ester

Chemical Property:

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Technology Process of 1-benzyl-2,6-dioxo-1,2,3,6-tetrahydropyridine-4-carboxylic acid ethyl ester

There total 1 articles about 1-benzyl-2,6-dioxo-1,2,3,6-tetrahydropyridine-4-carboxylic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: 623-91-6
diethyl Fumarate

: 330173-08-5
N-benzyl-2-(4-methylphenylsulfonyl)acetamide

: 503545-00-4
1-benzyl-2,6-dioxo-1,2,3,6-tetrahydropyridine-4-carboxylic acid ethyl ester

Guidance literature:: N-benzyl-2-(4-methylphenylsulfonyl)acetamide; With sodium hydride; In tetrahydrofuran; at 20 ℃; for 0.25h;

diethyl Fumarate; In tetrahydrofuran; for 0.5h; Heating;

Reference yield:

: 503545-00-4
1-benzyl-2,6-dioxo-1,2,3,6-tetrahydropyridine-4-carboxylic acid ethyl ester

: 158984-76-0
1,2,3,6-tetrahydro-1-(phenylmethyl)-4-pyridinemethanol

Guidance literature:: With lithium aluminium tetrahydride; aluminium trichloride; In tetrahydrofuran; 0 deg C, 30 min; reflux, 2 h;

Reference yield:

: 503545-00-4
1-benzyl-2,6-dioxo-1,2,3,6-tetrahydropyridine-4-carboxylic acid ethyl ester

: 503544-95-4
1-benzyl-1,2,3,6-tetrahydropyridine-4-carbaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: 162 mg / LAH; aluminum chloride / tetrahydrofuran / 0 deg C, 30 min; reflux, 2 h

2: 69 percent / oxalyl chloride; dimethyl sulfoxide / CH₂Cl₂ / 0.33 h / -78 °C

With lithium aluminium tetrahydride; aluminium trichloride; oxalyl dichloride; dimethyl sulfoxide; In tetrahydrofuran; dichloromethane; 2: Swern oxidation;