1-(2-benzoylethyl)-4-(2,3,4-trimethoxybenzyl)piperazine dihydrochloride

Base Information

Chemical Name:1-(2-benzoylethyl)-4-(2,3,4-trimethoxybenzyl)piperazine dihydrochloride
CAS No.:76925-14-9
Molecular Formula:C₂₃H₃₀N₂O₄*2ClH
Molecular Weight:471.424
Hs Code.:

Synonyms:1-(2-benzoylethyl)-4-(2,3,4-trimethoxybenzyl)piperazine dihydrochloride

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Chemical Property of 1-(2-benzoylethyl)-4-(2,3,4-trimethoxybenzyl)piperazine dihydrochloride

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Technology Process of 1-(2-benzoylethyl)-4-(2,3,4-trimethoxybenzyl)piperazine dihydrochloride

There total 1 articles about 1-(2-benzoylethyl)-4-(2,3,4-trimethoxybenzyl)piperazine dihydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 13171-25-0,127881-54-3
trimetazidine dihydrochloride

: 98-86-2
acetophenone

: 76925-14-9
1-(2-benzoylethyl)-4-(2,3,4-trimethoxybenzyl)piperazine dihydrochloride

Guidance literature:: In ethanol; for 6h; Heating;
DOI:10.1248/cpb.35.2774

Reference yield: 76.0%

: 76925-14-9
1-(2-benzoylethyl)-4-(2,3,4-trimethoxybenzyl)piperazine dihydrochloride

: 76924-96-4
1-Phenyl-3-[4-(2,3,4-trimethoxy-benzyl)-piperazin-1-yl]-propan-1-ol; hydrochloride

Guidance literature:: With sodium tetrahydroborate; In methanol; for 0.5h; Ambient temperature;
DOI:10.1248/cpb.35.2774

Reference yield:

: 76925-14-9
1-(2-benzoylethyl)-4-(2,3,4-trimethoxybenzyl)piperazine dihydrochloride

: 64966-11-6
1-((E)-3-Phenyl-allyl)-4-(2,3,4-trimethoxy-benzyl)-piperazine; hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / sodium borohydride (NaBH₄) / methanol / 0.5 h / Ambient temperature

2: 26 percent / phosphoric acid (50percent) / 7 h / 90 °C

With sodium tetrahydroborate; phosphoric acid; In methanol;
DOI:10.1248/cpb.35.2774