bromodiethylphenylgermane

Base Information

Chemical Name:bromodiethylphenylgermane
CAS No.:22949-92-4
Molecular Formula:C₁₀H₁₅BrGe
Molecular Weight:287.723
Hs Code.:

Synonyms:bromodiethylphenylgermane

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Chemical Property of bromodiethylphenylgermane

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Technology Process of bromodiethylphenylgermane

There total 1 articles about bromodiethylphenylgermane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 2945-43-9
Diethyldiphenylgermane

: 22949-92-4
bromodiethylphenylgermane

Guidance literature:: With bromine; In further solvent(s); addn. of bromine in 1,2-dibromoethane to Ge-compound in 1,2-dibromoethane at 80-85°C; refluxing for 2 h;; removal of solvent under reduced pressure; fractional distn.;;
DOI:10.1246/bcsj.59.2807

Reference yield: 83.0%

: 16853-85-3
lithium aluminium tetrahydride

: 22949-92-4
bromodiethylphenylgermane

: 79301-90-9
phenyldiethylgermane

Guidance literature:: In diethyl ether; slow addn. of the germane in dry ether to LiAlH4 in ether with stirring; refluxing for 2 h; quenching by slow addn. of water with cooling followed by sulfuric acid; organic layer was sepd. and dried over sodium sulfate; removal of solvent under reduced pressure; fractional distn.;;
DOI:10.1246/bcsj.59.2807

Reference yield: 48.0%

: 3761-92-0
n-hexylmagnesium bromide

: 22949-92-4
bromodiethylphenylgermane

: 109827-46-5
1-(diethylphenylgermyl)hexane

Guidance literature:: In tetrahydrofuran; addn. of the germane in THF to the Grignard compound in THF prepd. from1-bromohexane and Mg; refluxing for one night;; hydrolyzed with ice and water; sepn. of THF layer and extn. of aq. layer with ether; org. solns. were evapd.; chromy. (silica gel); fractional distn.;;
DOI:10.1246/bcsj.59.2807