diethyl(diphenyl)germane

Base Information

Chemical Name:diethyl(diphenyl)germane
CAS No.:2945-43-9
Molecular Formula:C₁₆H₂₀Ge
Molecular Weight:284.925
Hs Code.:

Synonyms:Diethyldiphenylgermane

Suppliers and Price of diethyl(diphenyl)germane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of diethyl(diphenyl)germane

Chemical Property:

Vapor Pressure:0.000419mmHg at 25°C

Purity/Quality:

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Technology Process of diethyl(diphenyl)germane

There total 7 articles about diethyl(diphenyl)germane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.1%

: 100184-59-6
diphenylgermylenedipotassium

: 75-00-3
chloroethane

: 1675-58-7
diphenylgermane

: 2945-43-9
Diethyldiphenylgermane

: 72454-22-9
Ethyldiphenylgermane

Guidance literature:: With water; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; soln. of Ph2GeK2 in HMPA/THF added to EtCl, stirred at room temp. for 30 min, cooled with water bath, hydrolyzed; extd. with ether, org. layer dried over anhyd. Na2SO4, isolated by preparative GLC and TLC;
DOI:10.1246/bcsj.58.1443

Reference yield: 60.1%

: 75-00-3
chloroethane

: (diphenylgermylene)dipotassium

: 2945-43-9
Diethyldiphenylgermane

: 72454-22-9
Ethyldiphenylgermane

Guidance literature:: In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; for 0.5h; Product distribution; Ambient temperature;
DOI:10.1246/bcsj.58.1443

Reference yield: 32.7%

: 100184-59-6
diphenylgermylenedipotassium

: 75-03-6
ethyl iodide

: 1675-58-7
diphenylgermane

: 2945-43-9
Diethyldiphenylgermane

: 72454-22-9
Ethyldiphenylgermane

Guidance literature:: With water; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; soln. of Ph2GeK2 in HMPA/THF added to EtI, stirred at room temp. for 30min, cooled with water bath, hydrolyzed; extd. with ether, org. layer dried over anhyd. Na2SO4, isolated by preparative GLC and TLC;
DOI:10.1246/bcsj.58.1443