2-tert-butoxycarbonylamino-3-phenyl-propionic acid 4,6-dimethoxy-[1,3,5]triazin-2-yl ester

Base Information

• Chemical Name: 2-tert-butoxycarbonylamino-3-phenyl-propionic acid 4,6-dimethoxy-[1,3,5]triazin-2-yl ester
• CAS No.: 1025839-59-1
• Molecular Formula: C₁₉H₂₄N₄O₆
• Molecular Weight: 404.423

Synonyms:2-tert-butoxycarbonylamino-3-phenyl-propionic acid 4,6-dimethoxy-[1,3,5]triazin-2-yl ester

Chemical Property of 2-tert-butoxycarbonylamino-3-phenyl-propionic acid 4,6-dimethoxy-[1,3,5]triazin-2-yl ester

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

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MSDS Files:

SDS file from LookChem

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Technology Process of 2-tert-butoxycarbonylamino-3-phenyl-propionic acid 4,6-dimethoxy-[1,3,5]triazin-2-yl ester

There total 2 articles about 2-tert-butoxycarbonylamino-3-phenyl-propionic acid 4,6-dimethoxy-[1,3,5]triazin-2-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

N-tert-butoxycarbonyl-L-phenylalanine (13734-34-4) + 4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride (3945-69-5) → 2-tert-butoxycarbonylamino-3-phenyl-propionic acid 4,6-dimethoxy-[1,3,5]triazin-2-yl ester (1025839-59-1)

Guidance literature:

In 1,2-dimethoxyethane; at 0 ℃; for 3h;

DOI:10.1021/jo991112f

Reference yield:

2-chloro-4,6-dimethoxy-1 ,3,5-triazine (3140-73-6) + N-tert-butoxycarbonyl-L-phenylalanine (13734-34-4) → 2-tert-butoxycarbonylamino-3-phenyl-propionic acid 4,6-dimethoxy-[1,3,5]triazin-2-yl ester (1025839-59-1)

Guidance literature:

With 4-methyl-morpholine; In tetrahydrofuran; at 20 ℃; for 0.5h; Inert atmosphere;

DOI:10.1039/c1ob06055d

Reference yield: 85.0%

2-tert-butoxycarbonylamino-3-phenyl-propionic acid 4,6-dimethoxy-[1,3,5]triazin-2-yl ester (1025839-59-1) → (S)-N-tert-butoxycarbonyl-2-amino-3-phenylpropanol (66605-57-0)

Guidance literature:

With hydrogen; palladium on activated charcoal; In 1,2-dimethoxyethane; at 20 ℃; for 3h; under 3800 Torr;

DOI:10.1021/jo991112f

upstream raw materials:

N-tert-butoxycarbonyl-L-phenylalanine

4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride

2-chloro-4,6-dimethoxy-1 ,3,5-triazine

Downstream raw materials:

Boc-L-phenylalaninal

(S)-N-tert-butoxycarbonyl-2-amino-3-phenylpropanol

(S)-tert-butyl 1-(3-(methylthiomethyl)-1,2,4-oxadiazol-5-yl)-2-phenylethylcarbamate

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