(2,3,4,5-tetrahydro-1,3a,6,8-tetraazaphenalene-1,6-diyl)bis(phenylmethanone)

Base Information

Chemical Name:(2,3,4,5-tetrahydro-1,3a,6,8-tetraazaphenalene-1,6-diyl)bis(phenylmethanone)
CAS No.:1262533-73-2
Molecular Formula:C₂₃H₂₀N₄O₂
Molecular Weight:384.437
Hs Code.:

Synonyms:(2,3,4,5-tetrahydro-1,3a,6,8-tetraazaphenalene-1,6-diyl)bis(phenylmethanone)

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Chemical Property of (2,3,4,5-tetrahydro-1,3a,6,8-tetraazaphenalene-1,6-diyl)bis(phenylmethanone)

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Technology Process of (2,3,4,5-tetrahydro-1,3a,6,8-tetraazaphenalene-1,6-diyl)bis(phenylmethanone)

There total 9 articles about (2,3,4,5-tetrahydro-1,3a,6,8-tetraazaphenalene-1,6-diyl)bis(phenylmethanone) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 927385-22-6
2,3,5,6-tetrahydro-1H,4H-1,3a,6,8-tetraaza-phenalene

: 98-88-4
benzoyl chloride

: 1262533-73-2
(2,3,4,5-tetrahydro-1,3a,6,8-tetraazaphenalene-1,6-diyl)bis(phenylmethanone)

Guidance literature:: With pyridine; at 0 - 20 ℃; for 6h; Inert atmosphere;
DOI:10.1021/ol1029589

Reference yield: 85.0%

: 927385-22-6
2,3,5,6-tetrahydro-1H,4H-1,3a,6,8-tetraaza-phenalene

: 93-97-0
benzoic acid anhydride

: 1262533-73-2
(2,3,4,5-tetrahydro-1,3a,6,8-tetraazaphenalene-1,6-diyl)bis(phenylmethanone)

Guidance literature:: With pyridine; at 170 ℃; for 1h; Microwave irradiation; Inert atmosphere;
DOI:10.1002/chem.201204452

Reference yield:

: 1262533-66-3
N,N-bis(2-chloroethyl)-3,5-dinitropyridin-4-amine

: 1262533-73-2
(2,3,4,5-tetrahydro-1,3a,6,8-tetraazaphenalene-1,6-diyl)bis(phenylmethanone)

Guidance literature:: Multi-step reaction with 2 steps

1: palladium 10% on activated carbon; hydrogen; potassium carbonate / ethanol / 48 h

2: pyridine / 6 h / 0 - 20 °C / Inert atmosphere

With pyridine; palladium 10% on activated carbon; hydrogen; potassium carbonate; In ethanol;
DOI:10.1021/ol1029589