N-[1-cyano-1-methyl-2-(5-cyano-2-{2-chloro-4-trifluoromethoxy-phenoxy}-phenoxy)-ethyl]-4-trifluoromethylsulfanylbenzamide

Base Information

Chemical Name:N-[1-cyano-1-methyl-2-(5-cyano-2-{2-chloro-4-trifluoromethoxy-phenoxy}-phenoxy)-ethyl]-4-trifluoromethylsulfanylbenzamide
CAS No.:1309111-21-4
Molecular Formula:C₂₆H₁₆ClF₆N₃O₄S
Molecular Weight:615.94
Hs Code.:

Synonyms:N-[1-cyano-1-methyl-2-(5-cyano-2-{2-chloro-4-trifluoromethoxy-phenoxy}-phenoxy)-ethyl]-4-trifluoromethylsulfanylbenzamide

Suppliers and Price of N-[1-cyano-1-methyl-2-(5-cyano-2-{2-chloro-4-trifluoromethoxy-phenoxy}-phenoxy)-ethyl]-4-trifluoromethylsulfanylbenzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N-[1-cyano-1-methyl-2-(5-cyano-2-{2-chloro-4-trifluoromethoxy-phenoxy}-phenoxy)-ethyl]-4-trifluoromethylsulfanylbenzamide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N-[1-cyano-1-methyl-2-(5-cyano-2-{2-chloro-4-trifluoromethoxy-phenoxy}-phenoxy)-ethyl]-4-trifluoromethylsulfanylbenzamide

There total 5 articles about N-[1-cyano-1-methyl-2-(5-cyano-2-{2-chloro-4-trifluoromethoxy-phenoxy}-phenoxy)-ethyl]-4-trifluoromethylsulfanylbenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 243128-37-2
4-fluoro-3-methoxybenzonitrile

: 1309111-21-4
N-[1-cyano-1-methyl-2-(5-cyano-2-{2-chloro-4-trifluoromethoxy-phenoxy}-phenoxy)-ethyl]-4-trifluoromethylsulfanylbenzamide

Guidance literature:: Multi-step reaction with 5 steps

1.1: caesium carbonate / N,N-dimethyl-formamide / 16 h / 120 °C

2.1: boron tribromide / dichloromethane / 20.5 h / 10 - 20 °C

2.2: Cooling with ice

3.1: potassium carbonate; potassium iodide / acetone / 4 h / Reflux

4.1: ammonia; ammonium chloride / ethanol; water / 16 h / 20 °C

5.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 20 h / 20 °C

With ammonia; boron tribromide; potassium carbonate; ammonium chloride; caesium carbonate; N-ethyl-N,N-diisopropylamine; potassium iodide; In ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetone;

Reference yield:

: 70783-75-4
4-(trifluoromethoxy)-2-chlorophenol

: 1309111-21-4
N-[1-cyano-1-methyl-2-(5-cyano-2-{2-chloro-4-trifluoromethoxy-phenoxy}-phenoxy)-ethyl]-4-trifluoromethylsulfanylbenzamide

Guidance literature:: Multi-step reaction with 5 steps

1.1: caesium carbonate / N,N-dimethyl-formamide / 16 h / 120 °C

2.1: boron tribromide / dichloromethane / 20.5 h / 10 - 20 °C

2.2: Cooling with ice

3.1: potassium carbonate; potassium iodide / acetone / 4 h / Reflux

4.1: ammonia; ammonium chloride / ethanol; water / 16 h / 20 °C

5.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 20 h / 20 °C

With ammonia; boron tribromide; potassium carbonate; ammonium chloride; caesium carbonate; N-ethyl-N,N-diisopropylamine; potassium iodide; In ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetone;

Reference yield:

: 1309111-06-5
4-{2-chloro-4-trifluoromethoxy-phenoxy}-3-methoxy-benzonitrile

: 1309111-21-4
N-[1-cyano-1-methyl-2-(5-cyano-2-{2-chloro-4-trifluoromethoxy-phenoxy}-phenoxy)-ethyl]-4-trifluoromethylsulfanylbenzamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: boron tribromide / dichloromethane / 20.5 h / 10 - 20 °C

1.2: Cooling with ice

2.1: potassium carbonate; potassium iodide / acetone / 4 h / Reflux

3.1: ammonia; ammonium chloride / ethanol; water / 16 h / 20 °C

4.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 20 h / 20 °C

With ammonia; boron tribromide; potassium carbonate; ammonium chloride; N-ethyl-N,N-diisopropylamine; potassium iodide; In ethanol; dichloromethane; water; acetone;