N-[1-cyano-1-methyl-2-(5-cyano-2-{2-chloro-4-trifluoromethoxy-phenoxy}-phenoxy)-ethyl]-4-trifluoromethylsulfonylbenzamide

Base Information

Chemical Name:N-[1-cyano-1-methyl-2-(5-cyano-2-{2-chloro-4-trifluoromethoxy-phenoxy}-phenoxy)-ethyl]-4-trifluoromethylsulfonylbenzamide
CAS No.:1309111-23-6
Molecular Formula:C₂₆H₁₆ClF₆N₃O₆S
Molecular Weight:647.939
Hs Code.:

Synonyms:N-[1-cyano-1-methyl-2-(5-cyano-2-{2-chloro-4-trifluoromethoxy-phenoxy}-phenoxy)-ethyl]-4-trifluoromethylsulfonylbenzamide

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Chemical Property of N-[1-cyano-1-methyl-2-(5-cyano-2-{2-chloro-4-trifluoromethoxy-phenoxy}-phenoxy)-ethyl]-4-trifluoromethylsulfonylbenzamide

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Technology Process of N-[1-cyano-1-methyl-2-(5-cyano-2-{2-chloro-4-trifluoromethoxy-phenoxy}-phenoxy)-ethyl]-4-trifluoromethylsulfonylbenzamide

There total 6 articles about N-[1-cyano-1-methyl-2-(5-cyano-2-{2-chloro-4-trifluoromethoxy-phenoxy}-phenoxy)-ethyl]-4-trifluoromethylsulfonylbenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1309111-21-4
N-[1-cyano-1-methyl-2-(5-cyano-2-{2-chloro-4-trifluoromethoxy-phenoxy}-phenoxy)-ethyl]-4-trifluoromethylsulfanylbenzamide

: 1309111-23-6
N-[1-cyano-1-methyl-2-(5-cyano-2-{2-chloro-4-trifluoromethoxy-phenoxy}-phenoxy)-ethyl]-4-trifluoromethylsulfonylbenzamide

Guidance literature:: With sodium periodate; ruthenium trichloride; In tetrachloromethane; water; acetonitrile; at 20 ℃; for 1.5h;

Reference yield:

: 243128-37-2
4-fluoro-3-methoxybenzonitrile

: 1309111-23-6
N-[1-cyano-1-methyl-2-(5-cyano-2-{2-chloro-4-trifluoromethoxy-phenoxy}-phenoxy)-ethyl]-4-trifluoromethylsulfonylbenzamide

Guidance literature:: Multi-step reaction with 6 steps

1.1: caesium carbonate / N,N-dimethyl-formamide / 16 h / 120 °C

2.1: boron tribromide / dichloromethane / 20.5 h / 10 - 20 °C

2.2: Cooling with ice

3.1: potassium carbonate; potassium iodide / acetone / 4 h / Reflux

4.1: ammonia; ammonium chloride / ethanol; water / 16 h / 20 °C

5.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 20 h / 20 °C

6.1: sodium periodate / ruthenium trichloride / tetrachloromethane; acetonitrile; water / 1.5 h / 20 °C

With sodium periodate; ammonia; boron tribromide; potassium carbonate; ammonium chloride; caesium carbonate; N-ethyl-N,N-diisopropylamine; potassium iodide; ruthenium trichloride; In tetrachloromethane; ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetone; acetonitrile;

Reference yield:

: 70783-75-4
4-(trifluoromethoxy)-2-chlorophenol

: 1309111-23-6
N-[1-cyano-1-methyl-2-(5-cyano-2-{2-chloro-4-trifluoromethoxy-phenoxy}-phenoxy)-ethyl]-4-trifluoromethylsulfonylbenzamide

Guidance literature:: Multi-step reaction with 6 steps

1.1: caesium carbonate / N,N-dimethyl-formamide / 16 h / 120 °C

2.1: boron tribromide / dichloromethane / 20.5 h / 10 - 20 °C

2.2: Cooling with ice

3.1: potassium carbonate; potassium iodide / acetone / 4 h / Reflux

4.1: ammonia; ammonium chloride / ethanol; water / 16 h / 20 °C

5.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 20 h / 20 °C

6.1: sodium periodate / ruthenium trichloride / tetrachloromethane; acetonitrile; water / 1.5 h / 20 °C

With sodium periodate; ammonia; boron tribromide; potassium carbonate; ammonium chloride; caesium carbonate; N-ethyl-N,N-diisopropylamine; potassium iodide; ruthenium trichloride; In tetrachloromethane; ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetone; acetonitrile;