1,3-Dichloro-2-[(E)-2-nitroethenyl]benzene

Base Information

Chemical Name:1,3-Dichloro-2-[(E)-2-nitroethenyl]benzene
CAS No.:52287-52-2
Molecular Formula:C₈H₅Cl₂NO₂
Molecular Weight:218.039
Hs Code.:
NSC Number:122864
DSSTox Substance ID:DTXSID901259978
Nikkaji Number:J1.935.034G,J717.918I
Wikidata:Q76305521
ChEMBL ID:CHEMBL1703209

Synonyms:22482-43-5;1-(2,6-Dichlorophenyl)-2-nitroethylene;1,3-dichloro-2-(2-nitrovinyl)benzene;1,3-Dichloro-2-[(E)-2-nitroethenyl]benzene;2,6-Dichloro-omega-nitrostyrene;1,3-Dichloro-2-(2-nitroethenyl)benzene;2,6-Dichloro-beta-nitrostyrene;Styrene, 2,6-dichloro-beta-nitro-;NSC122864;NSC 122864;1-(2,6-Dichlorophenyl)-2-nitroethene;MLS002701978;52287-52-2;1-(3,4-Methylenedioxy)phenyl-2-nitroethene;Benzene, 1,3-dichloro-2-(2-nitroethenyl)-;1,3-Dichloro-2-[(1E)-2-nitroethenyl]benzene;Benzene,1,3-dichloro-2-(2-nitroethenyl)-;(E)-1,3-dichloro-2-(2-nitrovinyl)benzene;SCHEMBL7414256;beta-Nitro-2,6-dichlorostyrene;CHEMBL1703209;HMS561L15;VXNHQIKJDIOBEC-SNAWJCMRSA-N;2,6-Dichloro- beta -nitrostyrene;DTXSID901259978;Styrene,6-dichloro-.beta.-nitro-;2,6-Dichloro-.omega.-nitrostyrene;XAA48243;(E)-beta-Nitro-2,6-dichlorostyrene;ANM102864;MFCD00024821;AKOS009156540;CCG-237068;NSC-122864;Styrene, 2,6-dichloro-.beta.-nitro-;LS-29811;PS-11464;SMR001565555;1,3-dichloro-2-[(E)-2-nitrovinyl]benzene;CS-0323956;trans-2,6-Dichloro-beta-nitrostyrene, 97%;1,3-Dichloro-2-[(E)-2-nitroethenyl]benzene #;EN300-1967262;A816227;(2-(2,6-Dichlorophenyl)vinyl)(hydroxy)azane oxide;1,3-bis(chloranyl)-2-[(E)-2-nitroethenyl]benzene;J-014738

Suppliers and Price of 1,3-Dichloro-2-[(E)-2-nitroethenyl]benzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 1,3-Dichloro-2-[(E)-2-nitroethenyl]benzene

Chemical Property:

XLogP3:3.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:216.9697338
Heavy Atom Count:13
Complexity:205

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=C(C(=C1)Cl)C=C[N+](=O)[O-])Cl
Isomeric SMILES:C1=CC(=C(C(=C1)Cl)/C=C/[N+](=O)[O-])Cl

Technology Process of 1,3-Dichloro-2-[(E)-2-nitroethenyl]benzene

There total 7 articles about 1,3-Dichloro-2-[(E)-2-nitroethenyl]benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 75-52-5
nitromethane

: 83-38-5
2,6-dichlorobenzaldehyde

: 52287-52-2
(E)-1,3-dichloro-2-(2-nitroethenyl)benzene

Guidance literature:: With ammonium acetate; In acetic acid; for 2h; Heating;

Reference yield: 81.0%

: 1029580-46-8
1-(2,6-dichlorophenyl)-2-nitroethan-1-ol

: 52287-52-2
(E)-1,3-dichloro-2-(2-nitroethenyl)benzene

Guidance literature:: With methanesulfonyl chloride; triethylamine; In tetrahydrofuran; at 0 ℃; for 1.5h;

Reference yield: 74.0%

: 52287-52-2
(E)-1,3-dichloro-2-(2-nitroethenyl)benzene

Guidance literature:: With chloro-trimethyl-silane; copper(ll) sulfate pentahydrate; guanidine nitrate; In acetonitrile; at 0 - 20 ℃; Inert atmosphere;

With triethylamine; In acetonitrile; at 20 ℃; for 0.416667h; stereoselective reaction; Inert atmosphere;