2-(2-((4-bromobenzyl)oxy)acetyl)-1-(4-(tert-butyl)benzyl)-N-ethylhydrazinecarboxamide

Base Information

Chemical Name:2-(2-((4-bromobenzyl)oxy)acetyl)-1-(4-(tert-butyl)benzyl)-N-ethylhydrazinecarboxamide
CAS No.:1454928-10-9
Molecular Formula:C₂₃H₃₀BrN₃O₃
Molecular Weight:476.413
Hs Code.:

Synonyms:2-(2-((4-bromobenzyl)oxy)acetyl)-1-(4-(tert-butyl)benzyl)-N-ethylhydrazinecarboxamide

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Chemical Property of 2-(2-((4-bromobenzyl)oxy)acetyl)-1-(4-(tert-butyl)benzyl)-N-ethylhydrazinecarboxamide

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Technology Process of 2-(2-((4-bromobenzyl)oxy)acetyl)-1-(4-(tert-butyl)benzyl)-N-ethylhydrazinecarboxamide

There total 3 articles about 2-(2-((4-bromobenzyl)oxy)acetyl)-1-(4-(tert-butyl)benzyl)-N-ethylhydrazinecarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: 1454928-30-3
1-(4-(tert-butyl)benzyl)-N-ethylhydrazinecarboxamide monomethanesulfonate

: 82499-60-3
<(p-bromobenzyl)oxy>acetic acid

: 1454928-10-9
2-(2-((4-bromobenzyl)oxy)acetyl)-1-(4-(tert-butyl)benzyl)-N-ethylhydrazinecarboxamide

Guidance literature:: With N-ethyl-N,N-diisopropylamine; HATU; In N,N-dimethyl-formamide; at 20 ℃; for 14h;

Reference yield:

: 873-75-6
4-bromobenzenemethanol

: 1454928-10-9
2-(2-((4-bromobenzyl)oxy)acetyl)-1-(4-(tert-butyl)benzyl)-N-ethylhydrazinecarboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: caesium carbonate / N,N-dimethyl-formamide / 16 h / 20 °C

2: trifluoroacetic acid / dichloromethane / 18 h / 20 °C

3: HATU; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 14 h / 20 °C

With caesium carbonate; N-ethyl-N,N-diisopropylamine; HATU; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 1454928-09-6
tert-butyl 2-((4-bromobenzyl)oxy)acetate

: 1454928-10-9
2-(2-((4-bromobenzyl)oxy)acetyl)-1-(4-(tert-butyl)benzyl)-N-ethylhydrazinecarboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / dichloromethane / 18 h / 20 °C

2: HATU; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 14 h / 20 °C

With N-ethyl-N,N-diisopropylamine; HATU; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide;