1-(4-(tert-butyl)benzyl)-N-ethylhydrazinecarboxamide monomethanesulfonate

Base Information

Chemical Name:1-(4-(tert-butyl)benzyl)-N-ethylhydrazinecarboxamide monomethanesulfonate
CAS No.:1454928-30-3
Molecular Formula:CH₄O₃S*C₁₄H₂₃N₃O
Molecular Weight:345.463
Hs Code.:

Synonyms:1-(4-(tert-butyl)benzyl)-N-ethylhydrazinecarboxamide monomethanesulfonate

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Chemical Property of 1-(4-(tert-butyl)benzyl)-N-ethylhydrazinecarboxamide monomethanesulfonate

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Technology Process of 1-(4-(tert-butyl)benzyl)-N-ethylhydrazinecarboxamide monomethanesulfonate

There total 3 articles about 1-(4-(tert-butyl)benzyl)-N-ethylhydrazinecarboxamide monomethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 75-75-2,98527-29-8
methanesulfonic acid

: 1616372-81-6
tert-butyl 2-(4-(tert-butyl)benzyl)-2-(ethylcarbamoyl)hydrazinecarboxylate

: 1454928-30-3
1-(4-(tert-butyl)benzyl)-N-ethylhydrazinecarboxamide monomethanesulfonate

Guidance literature:: In dichloromethane; at 20 ℃; for 16h; Inert atmosphere;

Reference yield:

: 1616373-18-2
(E)-tert-butyl 2-(4-(tert-butyl)benzylidene)hydrazine-carboxylate

: 1454928-30-3
1-(4-(tert-butyl)benzyl)-N-ethylhydrazinecarboxamide monomethanesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: platinum(IV) oxide; hydrogen / isopropyl alcohol; ethyl acetate / 120 h / 2585.81 Torr

2: dichloromethane / 48 h / 20 °C / Inert atmosphere

3: dichloromethane / 16 h / 20 °C / Inert atmosphere

With platinum(IV) oxide; hydrogen; In dichloromethane; ethyl acetate; isopropyl alcohol;

Reference yield:

: 425675-81-6
tert-butyl 2-(4-(tert-butyl)benzyl)hydrazinecarboxylate

: 1454928-30-3
1-(4-(tert-butyl)benzyl)-N-ethylhydrazinecarboxamide monomethanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane / 48 h / 20 °C / Inert atmosphere

2: dichloromethane / 16 h / 20 °C / Inert atmosphere

In dichloromethane;