4-(t-butoxycarbonylphenylalanylamino)butanoic acid 2-trimethylsilylethyl ester

Base Information

Chemical Name:4-(t-butoxycarbonylphenylalanylamino)butanoic acid 2-trimethylsilylethyl ester
CAS No.:108826-69-3
Molecular Formula:C₂₃H₃₈N₂O₅Si
Molecular Weight:450.651
Hs Code.:

Synonyms:4-(t-butoxycarbonylphenylalanylamino)butanoic acid 2-trimethylsilylethyl ester

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Chemical Property of 4-(t-butoxycarbonylphenylalanylamino)butanoic acid 2-trimethylsilylethyl ester

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Technology Process of 4-(t-butoxycarbonylphenylalanylamino)butanoic acid 2-trimethylsilylethyl ester

There total 3 articles about 4-(t-butoxycarbonylphenylalanylamino)butanoic acid 2-trimethylsilylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 13734-34-4
N-tert-butoxycarbonyl-L-phenylalanine

: 108826-68-2
4-aminobutanoic acid 2-trimethylsilylethyl ester hydrochloride

: 108826-69-3
4-(t-butoxycarbonylphenylalanylamino)butanoic acid 2-trimethylsilylethyl ester

Guidance literature:: With benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide; at 4 ℃; for 16h;

Reference yield:

: 2916-68-9
2-(Trimethylsilyl)ethanol

: 108826-69-3
4-(t-butoxycarbonylphenylalanylamino)butanoic acid 2-trimethylsilylethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 74 percent / DCC / pyridine

2: H₂ / 10percent Pd-C / propan-2-ol; acetic acid

3: 72 percent / 1.) HOBt, DCC; 2.) DIEA / dimethylformamide / 16 h / 4 °C

With hydrogen; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; palladium on activated charcoal; In pyridine; acetic acid; N,N-dimethyl-formamide; isopropyl alcohol;

Reference yield:

: 108826-67-1
4-benzyloxycarbonylaminobutanoic acid 2-trimethylsilylethyl ester

: 108826-69-3
4-(t-butoxycarbonylphenylalanylamino)butanoic acid 2-trimethylsilylethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / 10percent Pd-C / propan-2-ol; acetic acid

2: 72 percent / 1.) HOBt, DCC; 2.) DIEA / dimethylformamide / 16 h / 4 °C

With hydrogen; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; palladium on activated charcoal; In acetic acid; N,N-dimethyl-formamide; isopropyl alcohol;