4-phenylalanylaminobutanoic acid 2-trimethylsilylethyl ester hydrochloride

Base Information

Chemical Name:4-phenylalanylaminobutanoic acid 2-trimethylsilylethyl ester hydrochloride
CAS No.:108826-70-6
Molecular Formula:C₁₈H₃₀N₂O₃Si*ClH
Molecular Weight:386.994
Hs Code.:

Synonyms:4-phenylalanylaminobutanoic acid 2-trimethylsilylethyl ester hydrochloride

Suppliers and Price of 4-phenylalanylaminobutanoic acid 2-trimethylsilylethyl ester hydrochloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 4-phenylalanylaminobutanoic acid 2-trimethylsilylethyl ester hydrochloride

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4-phenylalanylaminobutanoic acid 2-trimethylsilylethyl ester hydrochloride

There total 4 articles about 4-phenylalanylaminobutanoic acid 2-trimethylsilylethyl ester hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 108826-69-3
4-(t-butoxycarbonylphenylalanylamino)butanoic acid 2-trimethylsilylethyl ester

: 108826-70-6
4-phenylalanylaminobutanoic acid 2-trimethylsilylethyl ester hydrochloride

Guidance literature:: With hydrogenchloride; In ethyl acetate; for 0.5h; Ambient temperature;

Reference yield:

: 2916-68-9
2-(Trimethylsilyl)ethanol

: 108826-70-6
4-phenylalanylaminobutanoic acid 2-trimethylsilylethyl ester hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: 74 percent / DCC / pyridine

2: H₂ / 10percent Pd-C / propan-2-ol; acetic acid

3: 72 percent / 1.) HOBt, DCC; 2.) DIEA / dimethylformamide / 16 h / 4 °C

4: 76 percent / 3M HCl / ethyl acetate / 0.5 h / Ambient temperature

With hydrogenchloride; hydrogen; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; palladium on activated charcoal; In pyridine; acetic acid; ethyl acetate; N,N-dimethyl-formamide; isopropyl alcohol;

Reference yield:

: 108826-67-1
4-benzyloxycarbonylaminobutanoic acid 2-trimethylsilylethyl ester

: 108826-70-6
4-phenylalanylaminobutanoic acid 2-trimethylsilylethyl ester hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: H₂ / 10percent Pd-C / propan-2-ol; acetic acid

2: 72 percent / 1.) HOBt, DCC; 2.) DIEA / dimethylformamide / 16 h / 4 °C

3: 76 percent / 3M HCl / ethyl acetate / 0.5 h / Ambient temperature

With hydrogenchloride; hydrogen; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; palladium on activated charcoal; In acetic acid; ethyl acetate; N,N-dimethyl-formamide; isopropyl alcohol;