(3Z,6Z)-3,6-Bis-<(2,4,5-trimethoxy-3-methylphenyl)methylene>piperazinedione

Base Information

Chemical Name:(3Z,6Z)-3,6-Bis-<(2,4,5-trimethoxy-3-methylphenyl)methylene>piperazinedione
CAS No.:137043-30-2
Molecular Formula:C₂₆H₃₀N₂O₈
Molecular Weight:498.533
Hs Code.:

Synonyms:(3Z,6Z)-3,6-Bis-<(2,4,5-trimethoxy-3-methylphenyl)methylene>piperazinedione

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3Z,6Z)-3,6-Bis-<(2,4,5-trimethoxy-3-methylphenyl)methylene>piperazinedione

Chemical Property:

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Technology Process of (3Z,6Z)-3,6-Bis-<(2,4,5-trimethoxy-3-methylphenyl)methylene>piperazinedione

There total 4 articles about (3Z,6Z)-3,6-Bis-<(2,4,5-trimethoxy-3-methylphenyl)methylene>piperazinedione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 3027-05-2
N,N'-diacetylpiperazin-2,5-dione

: 60059-09-8
2,4,5-trimethoxy-3-methylbenzaldehyde

: 137043-30-2
(3Z,6Z)-3,6-Bis-<(2,4,5-trimethoxy-3-methylphenyl)methylene>piperazinedione

Guidance literature:: With caesium carbonate; In dimethyl sulfoxide; ethyl acetate; at 80 ℃;
DOI:10.1002/ejoc.201402487

Reference yield:

: 137023-15-5
1-Hydroxymethyl-2,4,5-trimethoxy-3-methylbenzene

: 137043-30-2
(3Z,6Z)-3,6-Bis-<(2,4,5-trimethoxy-3-methylphenyl)methylene>piperazinedione

Guidance literature:: Multi-step reaction with 2 steps

1: 94.9 percent / pyridinium chlorochromate, MgSO₄ / CH₂Cl₂ / 0.25 h / Heating

2: 64.3 percent / Cs₂CO₃ / dimethylformamide / 3 h / 80 °C

With magnesium sulfate; caesium carbonate; pyridinium chlorochromate; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)86518-2

Reference yield:

: 137023-21-3
2,4-Dimethoxy-3-methyl-5-acetoxymethylphenol

: 137043-30-2
(3Z,6Z)-3,6-Bis-<(2,4,5-trimethoxy-3-methylphenyl)methylene>piperazinedione

Guidance literature:: Multi-step reaction with 4 steps

1: 93.4 percent / K₂CO₃ / acetone / 36 h / Heating

2: 98.1 percent / NaOH / CH₂Cl₂; methanol / 0.17 h / Heating

3: 94.9 percent / pyridinium chlorochromate, MgSO₄ / CH₂Cl₂ / 0.25 h / Heating

4: 64.3 percent / Cs₂CO₃ / dimethylformamide / 3 h / 80 °C

With sodium hydroxide; magnesium sulfate; potassium carbonate; caesium carbonate; pyridinium chlorochromate; In methanol; dichloromethane; N,N-dimethyl-formamide; acetone;
DOI:10.1016/S0040-4020(01)86518-2