1-[9-(4-Chloro-phenyl)-4-hydrazino-7-methyl-pyrido[3',2':4,5]thieno[3,2-d]pyrimidin-8-yl]-ethanone

Base Information

Chemical Name:1-[9-(4-Chloro-phenyl)-4-hydrazino-7-methyl-pyrido[3',2':4,5]thieno[3,2-d]pyrimidin-8-yl]-ethanone
CAS No.:470456-13-4
Molecular Formula:C₁₈H₁₄ClN₅OS
Molecular Weight:383.861
Hs Code.:

Synonyms:1-[9-(4-Chloro-phenyl)-4-hydrazino-7-methyl-pyrido[3',2':4,5]thieno[3,2-d]pyrimidin-8-yl]-ethanone

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Chemical Property of 1-[9-(4-Chloro-phenyl)-4-hydrazino-7-methyl-pyrido[3',2':4,5]thieno[3,2-d]pyrimidin-8-yl]-ethanone

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Technology Process of 1-[9-(4-Chloro-phenyl)-4-hydrazino-7-methyl-pyrido[3',2':4,5]thieno[3,2-d]pyrimidin-8-yl]-ethanone

There total 5 articles about 1-[9-(4-Chloro-phenyl)-4-hydrazino-7-methyl-pyrido[3',2':4,5]thieno[3,2-d]pyrimidin-8-yl]-ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 470456-00-9
1-[4-Chloro-9-(4-chloro-phenyl)-7-methyl-pyrido[3',2':4,5]thieno[3,2-d]pyrimidin-8-yl]-ethanone

: 470456-13-4
1-[9-(4-Chloro-phenyl)-4-hydrazino-7-methyl-pyrido[3',2':4,5]thieno[3,2-d]pyrimidin-8-yl]-ethanone

Guidance literature:: With hydrazine hydrate; In ethanol; for 2h; Heating;
DOI:10.1002/jccs.200200035

Reference yield:

: 103868-29-7
5-acetyl-6-methyl-4-(4-chlorophenyl)-3-cyano-2<1H>pyridinethione

: 470456-13-4
1-[9-(4-Chloro-phenyl)-4-hydrazino-7-methyl-pyrido[3',2':4,5]thieno[3,2-d]pyrimidin-8-yl]-ethanone

Guidance literature:: Multi-step reaction with 5 steps

1: 93 percent / CH₃CO₂Na*3H₂O / ethanol / 2 h / Heating

2: 92 percent / NaOEt / ethanol / 0.33 h / Heating

3: 89 percent / Ac₂O / 3 h / Heating

4: 87 percent / POCl₃ / 4 h / Heating

5: 92 percent / hydrazine hydrate / ethanol / 2 h / Heating

With sodium ethanolate; sodium acetate; acetic anhydride; hydrazine hydrate; trichlorophosphate; In ethanol;
DOI:10.1002/jccs.200200035

Reference yield:

: 470455-87-9
2-[5-acetyl-4-(4-chloro-phenyl)-3-cyano-6-methyl-pyridin-2-ylsulfanyl]-acetamide

: 470456-13-4
1-[9-(4-Chloro-phenyl)-4-hydrazino-7-methyl-pyrido[3',2':4,5]thieno[3,2-d]pyrimidin-8-yl]-ethanone

Guidance literature:: Multi-step reaction with 4 steps

1: 92 percent / NaOEt / ethanol / 0.33 h / Heating

2: 89 percent / Ac₂O / 3 h / Heating

3: 87 percent / POCl₃ / 4 h / Heating

4: 92 percent / hydrazine hydrate / ethanol / 2 h / Heating

With sodium ethanolate; acetic anhydride; hydrazine hydrate; trichlorophosphate; In ethanol;
DOI:10.1002/jccs.200200035