7-chloro-3-(2,6-dichlorophenyl)-3,4-dihydro-10-hydroxy-1,9(2H,10H)-acridinedione

Base Information

Chemical Name:7-chloro-3-(2,6-dichlorophenyl)-3,4-dihydro-10-hydroxy-1,9(2H,10H)-acridinedione
CAS No.:55579-52-7
Molecular Formula:C₁₉H₁₂Cl₃NO₃
Molecular Weight:408.668
Hs Code.:

Synonyms:7-chloro-3-(2,6-dichlorophenyl)-3,4-dihydro-10-hydroxy-1,9(2H,10H)-acridinedione

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 7-chloro-3-(2,6-dichlorophenyl)-3,4-dihydro-10-hydroxy-1,9(2H,10H)-acridinedione

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Technology Process of 7-chloro-3-(2,6-dichlorophenyl)-3,4-dihydro-10-hydroxy-1,9(2H,10H)-acridinedione

There total 6 articles about 7-chloro-3-(2,6-dichlorophenyl)-3,4-dihydro-10-hydroxy-1,9(2H,10H)-acridinedione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 55579-74-3
5-(2,6-dichlorophenyl)cyclohexane-1,3-dione

: 552-89-6
2-nitro-benzaldehyde

: 55579-52-7
7-chloro-3-(2,6-dichlorophenyl)-3,4-dihydro-10-hydroxy-1,9(2H,10H)-acridinedione

Guidance literature:: With hydrogenchloride; acetic acid; at 85 ℃; for 4h;
DOI:10.1021/jm00097a001

Reference yield:

: 83-38-5
2,6-dichlorobenzaldehyde

: 55579-52-7
7-chloro-3-(2,6-dichlorophenyl)-3,4-dihydro-10-hydroxy-1,9(2H,10H)-acridinedione

Guidance literature:: Multi-step reaction with 5 steps

1: 94 percent / 50percent aq. NaOH / 72 h / Ambient temperature

2: EtONa / ethanol / 6 h / Heating

3: 2 N NaOH / 2 h / Heating

4: 5 N H₂SO₄ / 4.5 h / Heating

5: 70 percent / concd HCl, glacial AcOH / 4 h / 85 °C

With hydrogenchloride; sodium hydroxide; sulfuric acid; sodium ethanolate; acetic acid; In ethanol;
DOI:10.1021/jm00097a001

Reference yield:

: 81559-89-9
4-(2,6-dichlorophenyl)-3-buten-2-one

: 55579-52-7
7-chloro-3-(2,6-dichlorophenyl)-3,4-dihydro-10-hydroxy-1,9(2H,10H)-acridinedione

Guidance literature:: Multi-step reaction with 4 steps

1: EtONa / ethanol / 6 h / Heating

2: 2 N NaOH / 2 h / Heating

3: 5 N H₂SO₄ / 4.5 h / Heating

4: 70 percent / concd HCl, glacial AcOH / 4 h / 85 °C

With hydrogenchloride; sodium hydroxide; sulfuric acid; sodium ethanolate; acetic acid; In ethanol;
DOI:10.1021/jm00097a001