9(2H)-Acridinone, 7-chloro-3-(2,6-dichlorophenyl)-1-[[3-(dimethylamino)propyl]imino]-1,3,4 ,10-tetrahydro-10-hydroxy-

Base Information

Chemical Name:9(2H)-Acridinone, 7-chloro-3-(2,6-dichlorophenyl)-1-[[3-(dimethylamino)propyl]imino]-1,3,4 ,10-tetrahydro-10-hydroxy-
CAS No.:144128-39-2
Molecular Formula:C₂₄H₂₄Cl₃N₃O₂
Molecular Weight:492.832
Hs Code.:
Mol file:144128-39-2.mol

Synonyms:

Suppliers and Price of 9(2H)-Acridinone, 7-chloro-3-(2,6-dichlorophenyl)-1-[[3-(dimethylamino)propyl]imino]-1,3,4 ,10-tetrahydro-10-hydroxy-

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 9(2H)-Acridinone, 7-chloro-3-(2,6-dichlorophenyl)-1-[[3-(dimethylamino)propyl]imino]-1,3,4 ,10-tetrahydro-10-hydroxy-

Chemical Property:

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Technology Process of 9(2H)-Acridinone, 7-chloro-3-(2,6-dichlorophenyl)-1-[[3-(dimethylamino)propyl]imino]-1,3,4 ,10-tetrahydro-10-hydroxy-

There total 6 articles about 9(2H)-Acridinone, 7-chloro-3-(2,6-dichlorophenyl)-1-[[3-(dimethylamino)propyl]imino]-1,3,4 ,10-tetrahydro-10-hydroxy- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 55579-52-7
7-chloro-3-(2,6-dichlorophenyl)-3,4-dihydro-10-hydroxy-1,9(2H,10H)-acridinedione

: 109-55-7
1-amino-3-(dimethylamino)propane

: 144128-39-2
7-Chloro-3-(2,6-dichloro-phenyl)-1-[(E)-3-dimethylamino-propylimino]-10-hydroxy-1,3,4,10-tetrahydro-2H-acridin-9-one

Guidance literature:: In ethanol; for 1.5h; Heating;
DOI:10.1021/jm00097a001

Reference yield:

: 83-38-5
2,6-dichlorobenzaldehyde

: 144128-39-2
7-Chloro-3-(2,6-dichloro-phenyl)-1-[(E)-3-dimethylamino-propylimino]-10-hydroxy-1,3,4,10-tetrahydro-2H-acridin-9-one

Guidance literature:: Multi-step reaction with 6 steps

1: 94 percent / 50percent aq. NaOH / 72 h / Ambient temperature

2: EtONa / ethanol / 6 h / Heating

3: 2 N NaOH / 2 h / Heating

4: 5 N H₂SO₄ / 4.5 h / Heating

5: 70 percent / concd HCl, glacial AcOH / 4 h / 85 °C

6: 65 percent / ethanol / 1.5 h / Heating

With hydrogenchloride; sodium hydroxide; sulfuric acid; sodium ethanolate; acetic acid; In ethanol;
DOI:10.1021/jm00097a001

Reference yield:

: 81559-89-9
4-(2,6-dichlorophenyl)-3-buten-2-one

: 144128-39-2
7-Chloro-3-(2,6-dichloro-phenyl)-1-[(E)-3-dimethylamino-propylimino]-10-hydroxy-1,3,4,10-tetrahydro-2H-acridin-9-one

Guidance literature:: Multi-step reaction with 5 steps

1: EtONa / ethanol / 6 h / Heating

2: 2 N NaOH / 2 h / Heating

3: 5 N H₂SO₄ / 4.5 h / Heating

4: 70 percent / concd HCl, glacial AcOH / 4 h / 85 °C

5: 65 percent / ethanol / 1.5 h / Heating

With hydrogenchloride; sodium hydroxide; sulfuric acid; sodium ethanolate; acetic acid; In ethanol;
DOI:10.1021/jm00097a001