(E)-1,3-di(p-methylbenzyl)-2-(2-methoxycarbonyl-1-phenylamino-1-propenyl)benzimidazolium chloride

Base Information

Chemical Name:(E)-1,3-di(p-methylbenzyl)-2-(2-methoxycarbonyl-1-phenylamino-1-propenyl)benzimidazolium chloride
CAS No.:1204110-65-5
Molecular Formula:C₃₄H₃₄N₃O₂*Cl
Molecular Weight:552.116
Hs Code.:

Synonyms:(E)-1,3-di(p-methylbenzyl)-2-(2-methoxycarbonyl-1-phenylamino-1-propenyl)benzimidazolium chloride

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Chemical Property of (E)-1,3-di(p-methylbenzyl)-2-(2-methoxycarbonyl-1-phenylamino-1-propenyl)benzimidazolium chloride

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Technology Process of (E)-1,3-di(p-methylbenzyl)-2-(2-methoxycarbonyl-1-phenylamino-1-propenyl)benzimidazolium chloride

There total 1 articles about (E)-1,3-di(p-methylbenzyl)-2-(2-methoxycarbonyl-1-phenylamino-1-propenyl)benzimidazolium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1093279-83-4
methyl 2-methyl-3-(phenylimino)acrylate

: 1204110-58-6
1,3?bis(4?methylbenzyl)benzimidazolium chloride

: 1204110-65-5
(E)-1,3-di(p-methylbenzyl)-2-(2-methoxycarbonyl-1-phenylamino-1-propenyl)benzimidazolium chloride

Guidance literature:: 1,3-di(4-methylbenzyl)-1H-benzo[d]imidazolium chloride; With potassium tert-butylate; In tetrahydrofuran; at -20 ℃; for 0.0833333h; Inert atmosphere;

methyl 2-methyl-3-(phenylimino)acrylate; In tetrahydrofuran; at -20 ℃; for 1h; Inert atmosphere;
DOI:10.1039/b915215f

Reference yield: 69.0%

: 1204110-65-5
(E)-1,3-di(p-methylbenzyl)-2-(2-methoxycarbonyl-1-phenylamino-1-propenyl)benzimidazolium chloride

: 762-42-5
dimethyl acetylenedicarboxylate

: 1204135-39-6
(E)-dimethyl 1,3-di(p-methylbenzyl)-2'-(1-methoxycarbonylethylidene)-1'-phenyl-1,1',2',3-tetrahydrospiro[benzimidazole-2,3'-pyrrole]-4',5'-dicarboxylate

Guidance literature:: (E)-1,3-di(p-methylbenzyl)-2-(2-methoxycarbonyl-1-phenylamino-1-propenyl)benzimidazolium chloride; With potassium tert-butylate; In toluene; at 20 - 80 ℃; Inert atmosphere;

dimethyl acetylenedicarboxylate; In toluene; at 80 ℃; for 0.5h; Inert atmosphere;
DOI:10.1039/b915215f

Reference yield: 61.0%

: 1204110-65-5
(E)-1,3-di(p-methylbenzyl)-2-(2-methoxycarbonyl-1-phenylamino-1-propenyl)benzimidazolium chloride

: 623-47-2
propynoic acid ethyl ester

: 1204110-78-0
(E)-ethyl 1,3-di(p-methylbenzyl)-2'-(1-methoxycarbonylethylidene)-1'-phenyl-1,1',2',3-tetrahydrospiro[benzimidazole-2,3'-pyrrole]-4'-carboxylate

Guidance literature:: (E)-1,3-di(p-methylbenzyl)-2-(2-methoxycarbonyl-1-phenylamino-1-propenyl)benzimidazolium chloride; With potassium tert-butylate; In toluene; at 20 - 80 ℃; Inert atmosphere;

propynoic acid ethyl ester; In toluene; at 80 ℃; for 0.5h; Inert atmosphere;
DOI:10.1039/b915215f