4-{[(S)-6,7-dihydro-2-nitro-5H-imidazo[2,1-b][1,3]oxazin-6-yloxy]methyl}benzaldehyde

Base Information

Chemical Name:4-{[(S)-6,7-dihydro-2-nitro-5H-imidazo[2,1-b][1,3]oxazin-6-yloxy]methyl}benzaldehyde
CAS No.:1415338-40-7
Molecular Formula:C₁₄H₁₃N₃O₅
Molecular Weight:303.274
Hs Code.:

Synonyms:4-{[(S)-6,7-dihydro-2-nitro-5H-imidazo[2,1-b][1,3]oxazin-6-yloxy]methyl}benzaldehyde

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Chemical Property of 4-{[(S)-6,7-dihydro-2-nitro-5H-imidazo[2,1-b][1,3]oxazin-6-yloxy]methyl}benzaldehyde

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Technology Process of 4-{[(S)-6,7-dihydro-2-nitro-5H-imidazo[2,1-b][1,3]oxazin-6-yloxy]methyl}benzaldehyde

There total 1 articles about 4-{[(S)-6,7-dihydro-2-nitro-5H-imidazo[2,1-b][1,3]oxazin-6-yloxy]methyl}benzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 187235-08-1
(S)‐2‐nitro‐6,7‐dihydro‐5H‐imidazo[2,1‐b][1,3]oxazin‐6‐ol

: 1122-91-4
4-bromo-benzaldehyde

: 1415338-40-7
4-{[(S)-6,7-dihydro-2-nitro-5H-imidazo[2,1-b][1,3]oxazin-6-yloxy]methyl}benzaldehyde

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 12.5h; Inert atmosphere;
DOI:10.1021/ml300362a

Reference yield: 63.0%

: 119072-55-8,7188-38-7
tert-butylisonitrile

: 1415338-40-7
4-{[(S)-6,7-dihydro-2-nitro-5H-imidazo[2,1-b][1,3]oxazin-6-yloxy]methyl}benzaldehyde

: 109-89-7
diethylamine

: 1415338-42-9
(4-{[(S)-6,7-dihydro-2-nitro-5H-imidazo[2,1-b][1,3]oxazin-6-yloxy]methyl}phenyl)(1-tert-butyl-1H-tetrazol-5-yl)-N,N-diethylmethanamine

Guidance literature:: 4-{[(S)-6,7-dihydro-2-nitro-5H-imidazo[2,1-b][1,3]oxazin-6-yloxy]methyl}benzaldehyde; diethylamine; In methanol; at 26 ℃; for 0.0833333h;

tert-butylisonitrile; With trimethylsilylazide; at 40 ℃; for 12h;
DOI:10.1021/ml300362a

Reference yield: 46.0%

: 119072-55-8,7188-38-7
tert-butylisonitrile

: 1415338-40-7
4-{[(S)-6,7-dihydro-2-nitro-5H-imidazo[2,1-b][1,3]oxazin-6-yloxy]methyl}benzaldehyde

: 124-40-3
dimethyl amine

: 1415338-41-8
(4-{[(S)-6,7-dihydro-2-nitro-5H-imidazo[2,1-b][1,3]oxazin-6-yloxy]methyl}phenyl)(1-tert-butyl-1H-tetrazol-5-yl)-N,N-dimethylmethanamine

Guidance literature:: 4-{[(S)-6,7-dihydro-2-nitro-5H-imidazo[2,1-b][1,3]oxazin-6-yloxy]methyl}benzaldehyde; dimethyl amine; In methanol; at 26 ℃; for 0.0833333h;

tert-butylisonitrile; With trimethylsilylazide; at 40 ℃; for 12h;
DOI:10.1021/ml300362a