phenylbis(trimethylsilyl)stibane

Base Information

Chemical Name:phenylbis(trimethylsilyl)stibane
CAS No.:82363-95-9
Molecular Formula:C₁₂H₂₃SbSi₂
Molecular Weight:345.236
Hs Code.:

Synonyms:phenylbis(trimethylsilyl)stibane

Suppliers and Price of phenylbis(trimethylsilyl)stibane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of phenylbis(trimethylsilyl)stibane

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of phenylbis(trimethylsilyl)stibane

There total 3 articles about phenylbis(trimethylsilyl)stibane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 75-77-4
chloro-trimethyl-silane

: 5035-52-9
dichlorophenylstibine

: 7439-95-4
magnesium

: 82363-95-9
phenylbis(trimethylsilyl)stibane

Guidance literature:: In tetrahydrofuran; byproducts: MgCl2; A soln. of PhSbCl2 in THF is added to Mg and Me3SiCl in THF, the mixture is stirred under Ar for 4 h.; evapn. of solvent under vac., residue is washed (petrolether), removal of solvent, distn. (80-90°C, 0.01 Torr);

Reference yield: 10.0%

: 75-77-4
chloro-trimethyl-silane

: 73046-27-2
dibromophenylantimony

: (C₆H₅)(n)

: 82363-95-9
phenylbis(trimethylsilyl)stibane

Guidance literature:: With magnesium; In tetrahydrofuran; byproducts: MgCl2, MgBr2; (Ar), Sb-compd. in THF added to Mg-chips, Me3SiCl added dropwise, stirred for 2 h; THF removed at 0.1 mmHg, washed several times with pentane, removed, distilled at 80°C/0.01 mmHg, elem. anal. (PhSb(SiMe3)2), pentane-insoluble part washed with water, dried, (PhSb)x pptd., elem. anal.;

Reference yield: 4.0%

: 75-77-4
chloro-trimethyl-silane

: 73046-27-2
dibromophenylantimony

: 82363-95-9
phenylbis(trimethylsilyl)stibane

: 82376-75-8
(C₆H₅)(Si(CH₃)3)SbSb(Si(CH₃)3)2

: 82363-97-1,82363-96-0
(C₆H₅SbSi(CH₃)3)2

Guidance literature:: With magnesium; In tetrahydrofuran; (Ar), soln. of the Si- and Sb-compd. droped to intensively stirred Mg-chips within 3 h at 22°C; volatiles removed at reduced pressure, washed several times with pentane, pentane removed, PhSb(SiMe3)2 distilled off;