benzyl 3-amino-6-(4-methylphenyl)pyrazine-2-carboxylate 4-oxide

Base Information

Chemical Name:benzyl 3-amino-6-(4-methylphenyl)pyrazine-2-carboxylate 4-oxide
CAS No.:113120-65-3
Molecular Formula:C₁₉H₁₇N₃O₃
Molecular Weight:335.362
Hs Code.:
Mol file:113120-65-3.mol

Synonyms:2-amino-3-benzyloxycarbonyl-5-(p-methylphenyl)pyrazine 1-oxide

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Chemical Property of benzyl 3-amino-6-(4-methylphenyl)pyrazine-2-carboxylate 4-oxide

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Technology Process of benzyl 3-amino-6-(4-methylphenyl)pyrazine-2-carboxylate 4-oxide

There total 3 articles about benzyl 3-amino-6-(4-methylphenyl)pyrazine-2-carboxylate 4-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 17628-76-1,1089298-03-2
p-tolylglyoxalmonoxime

: 59319-89-0
benzyl alpha-aminocyanoacetate methanesulfonic acid salt

: 113120-65-3
2-amino-3-benzyloxycarbonyl-5-(p-methylphenyl)pyrazine 1-oxide

Guidance literature:: In methanol; for 120h;

Reference yield:

: 1075-47-4
4-methylphenylglyoxal

: 113120-65-3
2-amino-3-benzyloxycarbonyl-5-(p-methylphenyl)pyrazine 1-oxide

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / acetonoxime, 2 N HCl / H₂O; methanol / 2 h / 50 °C / pH 4

2: 81 percent / methanol / 120 h

With hydrogenchloride; acetone oxime; In methanol; water;

Reference yield:

: 16208-14-3
2,2-dihydroxy-1-(p-tolyl)ethanone

: 113120-65-3
2-amino-3-benzyloxycarbonyl-5-(p-methylphenyl)pyrazine 1-oxide

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / acetonoxime, 2 N HCl / H₂O / 2 h / 50 °C / pH 4

2: 81 percent / methanol / 120 h

With hydrogenchloride; acetone oxime; In methanol; water;