4-tert-butylphenoxy[2,3,7,8,12,13-hexa(ethylthio)subporphyrazinato]boron(III)

Base Information

Chemical Name:4-tert-butylphenoxy[2,3,7,8,12,13-hexa(ethylthio)subporphyrazinato]boron(III)
CAS No.:1450813-54-3
Molecular Formula:C₃₄H₄₃BN₆OS₆
Molecular Weight:754.962
Hs Code.:

Synonyms:4-tert-butylphenoxy[2,3,7,8,12,13-hexa(ethylthio)subporphyrazinato]boron(III)

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Chemical Property of 4-tert-butylphenoxy[2,3,7,8,12,13-hexa(ethylthio)subporphyrazinato]boron(III)

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Technology Process of 4-tert-butylphenoxy[2,3,7,8,12,13-hexa(ethylthio)subporphyrazinato]boron(III)

There total 2 articles about 4-tert-butylphenoxy[2,3,7,8,12,13-hexa(ethylthio)subporphyrazinato]boron(III) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 14.0%

: 98-54-4
para-tert-butylphenol

: 10294-34-5
boron trichloride

: 70122-11-1
bis(ethylthio)maleonitrile

: 1450813-54-3
4-tert-butylphenoxy[2,3,7,8,12,13-hexa(ethylthio)subporphyrazinato]boron(III)

Guidance literature:: boron trichloride; bis(ethylthio)maleonitrile; In 5,5-dimethyl-1,3-cyclohexadiene; at 100 ℃; for 0.75h; Inert atmosphere;

para-tert-butylphenol; In toluene; for 2h; Inert atmosphere; Reflux;
DOI:10.1002/chem.201301140

Reference yield:

: 98-54-4
para-tert-butylphenol

: 70970-52-4
2,3-bis(ethylthio)maleonitrile

: 10294-34-5
boron trichloride

: 75-08-1
ethanethiol

: 1450813-54-3
4-tert-butylphenoxy[2,3,7,8,12,13-hexa(ethylthio)subporphyrazinato]boron(III)

: C₃₂H₃₈BClN₆OS₅

Guidance literature:: 2,3-bis(ethylthio)maleonitrile; boron trichloride; In para-xylene; at 110 ℃; for 1h; Inert atmosphere; Schlenk technique;

para-tert-butylphenol; In toluene; for 2h; Reflux; Inert atmosphere; Schlenk technique;

ethanethiol; With 1,3-dimethyl-2-imidazolidinone; triethylamine; at 0 - 20 ℃; for 1h; Inert atmosphere; Schlenk technique;
DOI:10.1021/acs.joc.9b02658

Reference yield: 43.0%

: 1450813-54-3
4-tert-butylphenoxy[2,3,7,8,12,13-hexa(ethylthio)subporphyrazinato]boron(III)

: 99768-12-4
4-methoxycarbonylphenylboronic acid

: 1450813-69-0
4-tert-butylphenoxy[2,3,7,8,12,13-hexa(4-methoxycarbonylphenyl)subporphyrazinato]boron(III)

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(I) thiophene-2-carboxylate; In tetrahydrofuran; at 60 ℃; for 20h; Inert atmosphere;
DOI:10.1002/chem.201301140