4-hydroxy-4-phenyl-2-butynyl methyl ether

Base Information Edit

Chemical Name:4-hydroxy-4-phenyl-2-butynyl methyl ether
CAS No.:32904-84-0
Molecular Formula:C₁₁H₁₂O₂
Molecular Weight:176.215
Hs Code.:
Mol file:32904-84-0.mol

Synonyms:4-hydroxy-4-phenyl-2-butynyl methyl ether

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-hydroxy-4-phenyl-2-butynyl methyl ether Edit

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Technology Process of 4-hydroxy-4-phenyl-2-butynyl methyl ether

There total 5 articles about 4-hydroxy-4-phenyl-2-butynyl methyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 73390-08-6
3-methoxy-1-propyn-1-yllithium

: 100-52-7
benzaldehyde

: 32904-84-0
4-hydroxy-4-phenyl-2-butynyl methyl ether

Guidance literature:: In tetrahydrofuran; at 0 ℃;

Reference yield: 60.0%

: 4187-87-5
1-Phenyl-2-propyn-1-ol

: 107-30-2
chloromethyl methyl ether

: 32904-84-0
4-hydroxy-4-phenyl-2-butynyl methyl ether

Guidance literature:: 1-Phenyl-2-propyn-1-ol; With n-butyllithium; In diethyl ether; hexane; at -78 ℃; for 0.633333h; Inert atmosphere;

chloromethyl methyl ether; In diethyl ether; hexane; at -78 - -30 ℃; Inert atmosphere;

With hydrogenchloride; In diethyl ether; hexane; water;
DOI:10.1016/j.tet.2009.02.061