O-(2,3,4-tri-O-benzoyl-α-D-glucopyranosyl)-(1<*>1)-2,3,4,6-tetra-O-benzoyl-α-D-glucopyranoside

Base Information

Chemical Name:O-(2,3,4-tri-O-benzoyl-α-D-glucopyranosyl)-(1<*>1)-2,3,4,6-tetra-O-benzoyl-α-D-glucopyranoside
CAS No.:146530-69-0
Molecular Formula:C₆₁H₅₀O₁₈
Molecular Weight:1071.06
Hs Code.:

Synonyms:O-(2,3,4-tri-O-benzoyl-α-D-glucopyranosyl)-(1<*>1)-2,3,4,6-tetra-O-benzoyl-α-D-glucopyranoside

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Chemical Property of O-(2,3,4-tri-O-benzoyl-α-D-glucopyranosyl)-(1<*>1)-2,3,4,6-tetra-O-benzoyl-α-D-glucopyranoside

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Technology Process of O-(2,3,4-tri-O-benzoyl-α-D-glucopyranosyl)-(1<*>1)-2,3,4,6-tetra-O-benzoyl-α-D-glucopyranoside

There total 4 articles about O-(2,3,4-tri-O-benzoyl-α-D-glucopyranosyl)-(1<*>1)-2,3,4,6-tetra-O-benzoyl-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 98-88-4
benzoyl chloride

: 142386-46-7
2,3,4,2',3',4'-hexakis-O-benzoyl-α,α-D-trehalose

: 146530-69-0
O-(2,3,4-tri-O-benzoyl-α-D-glucopyranosyl)-(1<*>1)-2,3,4,6-tetra-O-benzoyl-α-D-glucopyranoside

Guidance literature:: With dmap; In pyridine; at 20 ℃; for 12h;
DOI:10.1016/j.carres.2007.05.009

Reference yield:

: C₈₀H₆₄O₁₈

: 146530-69-0
O-(2,3,4-tri-O-benzoyl-α-D-glucopyranosyl)-(1<*>1)-2,3,4,6-tetra-O-benzoyl-α-D-glucopyranoside

Guidance literature:: With acetic acid; at 70 ℃; for 2h; Yield given;
DOI:10.1021/jo00057a021

Reference yield:

: 951165-32-5
6,6'-di-O-tert-butyldimethylsilyl-2,3,4,2',3',4'-hexa-O-benzoyl-α,α-D-trehalose

: 146530-69-0
O-(2,3,4-tri-O-benzoyl-α-D-glucopyranosyl)-(1<*>1)-2,3,4,6-tetra-O-benzoyl-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / TBAF / tetrahydrofuran; acetic acid / 24 h

2: DMAP / pyridine / 12 h / 20 °C

With dmap; tetrabutyl ammonium fluoride; In tetrahydrofuran; pyridine; acetic acid;
DOI:10.1016/j.carres.2007.05.009