(2S)-(2-bromo-benzoylamino)-(3R)-triisopropylsilanyloxybutyric acid methyl ester

Base Information

Chemical Name:(2S)-(2-bromo-benzoylamino)-(3R)-triisopropylsilanyloxybutyric acid methyl ester
CAS No.:716369-27-6
Molecular Formula:C₂₁H₃₄BrNO₄Si
Molecular Weight:472.495
Hs Code.:

Synonyms:(2S)-(2-bromo-benzoylamino)-(3R)-triisopropylsilanyloxybutyric acid methyl ester

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Chemical Property of (2S)-(2-bromo-benzoylamino)-(3R)-triisopropylsilanyloxybutyric acid methyl ester

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Technology Process of (2S)-(2-bromo-benzoylamino)-(3R)-triisopropylsilanyloxybutyric acid methyl ester

There total 2 articles about (2S)-(2-bromo-benzoylamino)-(3R)-triisopropylsilanyloxybutyric acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 80522-42-5
triisopropylsilyl trifluoromethanesulfonate

: 716369-25-4
(2S)-(2-bromo-benzoylamino)-(3R)-hydroxy-butyric acid methyl ester

: 716369-27-6
(2S)-(2-bromo-benzoylamino)-(3R)-triisopropylsilanyloxybutyric acid methyl ester

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃; for 3h;
DOI:10.1039/b316502g

Reference yield:

: 7154-66-7
2-bromobenzoic acid chloride

: 716369-27-6
(2S)-(2-bromo-benzoylamino)-(3R)-triisopropylsilanyloxybutyric acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 58 percent / Et₃N; DMAP / CH₂Cl₂ / 2 h / 0 - 20 °C

2: 62 percent / Et₃N / CH₂Cl₂ / 3 h / 0 - 20 °C

With dmap; triethylamine; In dichloromethane;
DOI:10.1039/b316502g