5-{4-[N-(tert-butyloxy)carbonyl]-4-[N,N-(dimethylamino)benzyl]amino}butylcarbamoylpentanohydroxamic acid

Base Information

• Chemical Name: 5-{4-[N-(tert-butyloxy)carbonyl]-4-[N,N-(dimethylamino)benzyl]amino}butylcarbamoylpentanohydroxamic acid
• CAS No.: 868836-08-2
• Molecular Formula: C₂₄H₄₀N₄O₅
• Molecular Weight: 464.605

Synonyms:5-{4-[N-(tert-butyloxy)carbonyl]-4-[N,N-(dimethylamino)benzyl]amino}butylcarbamoylpentanohydroxamic acid

Chemical Property of 5-{4-[N-(tert-butyloxy)carbonyl]-4-[N,N-(dimethylamino)benzyl]amino}butylcarbamoylpentanohydroxamic acid

Chemical Property:

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Technology Process of 5-{4-[N-(tert-butyloxy)carbonyl]-4-[N,N-(dimethylamino)benzyl]amino}butylcarbamoylpentanohydroxamic acid

There total 7 articles about 5-{4-[N-(tert-butyloxy)carbonyl]-4-[N,N-(dimethylamino)benzyl]amino}butylcarbamoylpentanohydroxamic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C27H43N3O7 → 5-{4-[N-(tert-butyloxy)carbonyl]-4-[N,N-(dimethylamino)benzyl]amino}butylcarbamoylpentanohydroxamic acid (868836-08-2)

Guidance literature:

With hydroxylamine; In tetrahydrofuran; methanol; at 20 ℃; for 0.5h;

Reference yield:

5-{4-[N-(tert-butyloxy)carbonyl]-4-[N,N-(dimethylamino)benzyl]amino}butylcarbamoylpentanoic acid (868836-03-7) → 5-{4-[N-(tert-butyloxy)carbonyl]-4-[N,N-(dimethylamino)benzyl]amino}butylcarbamoylpentanohydroxamic acid (868836-08-2)

Guidance literature:

5-{4-[N-(tert-butyloxy)carbonyl]-4-[N,N-(dimethylamino)benzyl]amino}butylcarbamoylpentanoic acid; With chloroformic acid ethyl ester; triethylamine; In tetrahydrofuran; at 0 ℃; for 0.333333h;

With hydroxylamine; In tetrahydrofuran; methanol; at 20 ℃; for 0.5h;

DOI:10.1021/jm0505009

Reference yield:

5-{4-[N-(tert-butyloxy)carbonyl]-4-[N,N-(dimethylamino)benzyl]amino}butylcarbamoylpentanoic acid methyl ester (868835-98-7) → 5-{4-[N-(tert-butyloxy)carbonyl]-4-[N,N-(dimethylamino)benzyl]amino}butylcarbamoylpentanohydroxamic acid (868836-08-2)

Guidance literature:

Multi-step reaction with 2 steps

1.1: aq. LiOH / tetrahydrofuran / 0 - 20 °C

2.1: ethyl chloroformate; triethylamine / tetrahydrofuran / 0.33 h / 0 °C

2.2: 0.252 g / hydroxylamine / methanol; tetrahydrofuran / 0.5 h / 20 °C

With lithium hydroxide; chloroformic acid ethyl ester; triethylamine; In tetrahydrofuran;

DOI:10.1021/jm0505009

upstream raw materials:

5-{4-[N-(tert-butyloxy)carbonyl]-4-[N,N-(dimethylamino)benzyl]amino}butylcarbamoylpentanoic acid

1-N-{4-[(N,N-dimethyl)amino]benzyl}-1-N-[(tert-butyloxy)carbonyl]-4-aminobutylamine

N-{4-[(N,N-dimethylamino)benzyl]butyl}phthalimide

1-N-{4-[(N,N-dimethyl)amino]benzyl}-1-N-[(tert-butyloxy)carbonyl]-4-phthalimidobutylamine

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