1-N-{4-[(N,N-dimethyl)amino]benzyl}-1-N-[(tert-butyloxy)carbonyl]-4-aminobutylamine

Base Information

Chemical Name:1-N-{4-[(N,N-dimethyl)amino]benzyl}-1-N-[(tert-butyloxy)carbonyl]-4-aminobutylamine
CAS No.:868835-94-3
Molecular Formula:C₁₈H₃₁N₃O₂
Molecular Weight:321.463
Hs Code.:

Synonyms:1-N-{4-[(N,N-dimethyl)amino]benzyl}-1-N-[(tert-butyloxy)carbonyl]-4-aminobutylamine

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Chemical Property of 1-N-{4-[(N,N-dimethyl)amino]benzyl}-1-N-[(tert-butyloxy)carbonyl]-4-aminobutylamine

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Technology Process of 1-N-{4-[(N,N-dimethyl)amino]benzyl}-1-N-[(tert-butyloxy)carbonyl]-4-aminobutylamine

There total 3 articles about 1-N-{4-[(N,N-dimethyl)amino]benzyl}-1-N-[(tert-butyloxy)carbonyl]-4-aminobutylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.3%

: 868835-91-0
1-N-{4-[(N,N-dimethyl)amino]benzyl}-1-N-[(tert-butyloxy)carbonyl]-4-phthalimidobutylamine

: 868835-94-3
1-N-{4-[(N,N-dimethyl)amino]benzyl}-1-N-[(tert-butyloxy)carbonyl]-4-aminobutylamine

Guidance literature:: With hydrazine; In methanol; for 12h; Heating;
DOI:10.1021/jm0505009

Reference yield:

: 868835-87-4
N-{4-[(N,N-dimethylamino)benzyl]butyl}phthalimide

: 868835-94-3
1-N-{4-[(N,N-dimethyl)amino]benzyl}-1-N-[(tert-butyloxy)carbonyl]-4-aminobutylamine

Guidance literature:: Multi-step reaction with 2 steps

1: aq. NaHCO₃; NaCl / CH₂Cl₂ / 12 h / Heating

2: 88.3 percent / hydrazine / methanol / 12 h / Heating

With sodium hydrogencarbonate; sodium chloride; hydrazine; In methanol; dichloromethane;
DOI:10.1021/jm0505009

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 868835-94-3
1-N-{4-[(N,N-dimethyl)amino]benzyl}-1-N-[(tert-butyloxy)carbonyl]-4-aminobutylamine

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydrogencarbonate; sodium chloride / dichloromethane; water / 0.5 h / 0 °C

1.2: 12.17 h / 0 - 20 °C / Heating / reflux

2.1: hydrazine / methanol / 12 h / Heating / reflux

With sodium hydrogencarbonate; sodium chloride; hydrazine; In methanol; dichloromethane; water;