[(2R)-N-(tert-Butoxycarbonyl)-α-methyl aspartyl]-β-(2S)-phenylalaninate ester

Base Information

Chemical Name:[(2R)-N-(tert-Butoxycarbonyl)-α-methyl aspartyl]-β-(2S)-phenylalaninate ester
CAS No.:196938-87-1
Molecular Formula:C₁₉H₂₆N₂O₇
Molecular Weight:394.425
Hs Code.:

Synonyms:[(2R)-N-(tert-Butoxycarbonyl)-α-methyl aspartyl]-β-(2S)-phenylalaninate ester

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Chemical Property of [(2R)-N-(tert-Butoxycarbonyl)-α-methyl aspartyl]-β-(2S)-phenylalaninate ester

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Technology Process of [(2R)-N-(tert-Butoxycarbonyl)-α-methyl aspartyl]-β-(2S)-phenylalaninate ester

There total 5 articles about [(2R)-N-(tert-Butoxycarbonyl)-α-methyl aspartyl]-β-(2S)-phenylalaninate ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 196938-86-0
Benzyl [(2R)-N-(tert-butoxycarbonyl)-α-methyl aspartyl]-β-(2S)-phenylalaninate diester

: 196938-87-1
[(2R)-N-(tert-Butoxycarbonyl)-α-methyl aspartyl]-β-(2S)-phenylalaninate ester

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; for 3h; Ambient temperature;

Reference yield:

: 51186-58-4,98482-77-0
4-benzyl Boc-D-aspartate

: 196938-87-1
[(2R)-N-(tert-Butoxycarbonyl)-α-methyl aspartyl]-β-(2S)-phenylalaninate ester

Guidance literature:: Multi-step reaction with 5 steps

1: 100 percent / diethyl ether / 0.5 h / 0 °C

2: 100 percent / H₂ / 10percent Pd/C / ethanol / 3 h / Ambient temperature

3: N-methylmorpholine / tetrahydrofuran / 0.08 h / -15 °C

4: N-methylmorpholine / tetrahydrofuran; dimethylformamide / 0.42 h / Ambient temperature

5: 100 percent / H₂ / 10percent Pd/C / ethanol / 3 h / Ambient temperature

With 4-methyl-morpholine; hydrogen; palladium on activated charcoal; In tetrahydrofuran; diethyl ether; ethanol; N,N-dimethyl-formamide;

Reference yield:

: 80963-12-8
α-Methyl β-benzyl (2R)-N-(tert-butoxycarbonyl)aspartate diester

: 196938-87-1
[(2R)-N-(tert-Butoxycarbonyl)-α-methyl aspartyl]-β-(2S)-phenylalaninate ester

Guidance literature:: Multi-step reaction with 4 steps

1: 100 percent / H₂ / 10percent Pd/C / ethanol / 3 h / Ambient temperature

2: N-methylmorpholine / tetrahydrofuran / 0.08 h / -15 °C

3: N-methylmorpholine / tetrahydrofuran; dimethylformamide / 0.42 h / Ambient temperature

4: 100 percent / H₂ / 10percent Pd/C / ethanol / 3 h / Ambient temperature

With 4-methyl-morpholine; hydrogen; palladium on activated charcoal; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide;