Benzyl [(2R)-N-(tert-butoxycarbonyl)-α-methyl aspartyl]-β-(2S)-phenylalaninate diester

Base Information

Chemical Name:Benzyl [(2R)-N-(tert-butoxycarbonyl)-α-methyl aspartyl]-β-(2S)-phenylalaninate diester
CAS No.:196938-86-0
Molecular Formula:C₂₆H₃₂N₂O₇
Molecular Weight:484.549
Hs Code.:

Synonyms:Benzyl [(2R)-N-(tert-butoxycarbonyl)-α-methyl aspartyl]-β-(2S)-phenylalaninate diester

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Chemical Property of Benzyl [(2R)-N-(tert-butoxycarbonyl)-α-methyl aspartyl]-β-(2S)-phenylalaninate diester

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Technology Process of Benzyl [(2R)-N-(tert-butoxycarbonyl)-α-methyl aspartyl]-β-(2S)-phenylalaninate diester

There total 4 articles about Benzyl [(2R)-N-(tert-butoxycarbonyl)-α-methyl aspartyl]-β-(2S)-phenylalaninate diester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 51186-58-4,98482-77-0
4-benzyl Boc-D-aspartate

: 196938-86-0
Benzyl [(2R)-N-(tert-butoxycarbonyl)-α-methyl aspartyl]-β-(2S)-phenylalaninate diester

Guidance literature:: Multi-step reaction with 4 steps

1: 100 percent / diethyl ether / 0.5 h / 0 °C

2: 100 percent / H₂ / 10percent Pd/C / ethanol / 3 h / Ambient temperature

3: N-methylmorpholine / tetrahydrofuran / 0.08 h / -15 °C

4: N-methylmorpholine / tetrahydrofuran; dimethylformamide / 0.42 h / Ambient temperature

With 4-methyl-morpholine; hydrogen; palladium on activated charcoal; In tetrahydrofuran; diethyl ether; ethanol; N,N-dimethyl-formamide;

Reference yield:

: 80963-12-8
α-Methyl β-benzyl (2R)-N-(tert-butoxycarbonyl)aspartate diester

: 196938-86-0
Benzyl [(2R)-N-(tert-butoxycarbonyl)-α-methyl aspartyl]-β-(2S)-phenylalaninate diester

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / H₂ / 10percent Pd/C / ethanol / 3 h / Ambient temperature

2: N-methylmorpholine / tetrahydrofuran / 0.08 h / -15 °C

3: N-methylmorpholine / tetrahydrofuran; dimethylformamide / 0.42 h / Ambient temperature

With 4-methyl-morpholine; hydrogen; palladium on activated charcoal; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide;

Reference yield:

: 98045-03-5,137130-65-5
(R)-3-(tert-butoxycarbonylamino)-4-methoxy-4-oxobutanoic acid

: 196938-86-0
Benzyl [(2R)-N-(tert-butoxycarbonyl)-α-methyl aspartyl]-β-(2S)-phenylalaninate diester

Guidance literature:: Multi-step reaction with 2 steps

1: N-methylmorpholine / tetrahydrofuran / 0.08 h / -15 °C

2: N-methylmorpholine / tetrahydrofuran; dimethylformamide / 0.42 h / Ambient temperature

With 4-methyl-morpholine; In tetrahydrofuran; N,N-dimethyl-formamide;