2-(o-tert-butyl phenylsulfonylcarbamate)-1-p-methoxyphenylethanone

Base Information

Chemical Name:2-(o-tert-butyl phenylsulfonylcarbamate)-1-p-methoxyphenylethanone
CAS No.:1309367-83-6
Molecular Formula:C₂₀H₂₃NO₆S
Molecular Weight:405.472
Hs Code.:

Synonyms:2-(o-tert-butyl phenylsulfonylcarbamate)-1-p-methoxyphenylethanone

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Chemical Property of 2-(o-tert-butyl phenylsulfonylcarbamate)-1-p-methoxyphenylethanone

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Technology Process of 2-(o-tert-butyl phenylsulfonylcarbamate)-1-p-methoxyphenylethanone

There total 3 articles about 2-(o-tert-butyl phenylsulfonylcarbamate)-1-p-methoxyphenylethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 960319-23-7
N-Boc-2-[2-hydroxy-2-(4-methoxyphenyl)ethyl]benzenesulfonamide

: 1309367-83-6
2-(o-tert-butyl phenylsulfonylcarbamate)-1-p-methoxyphenylethanone

Guidance literature:: With pyridinium chlorochromate; In dichloromethane; at 20 ℃;
DOI:10.1039/c1cc10313j

Reference yield:

: 123-11-5
4-methoxy-benzaldehyde

: 1309367-83-6
2-(o-tert-butyl phenylsulfonylcarbamate)-1-p-methoxyphenylethanone

Guidance literature:: Multi-step reaction with 2 steps

1: n-butyllithium

2: pyridinium chlorochromate / dichloromethane / 20 °C

With n-butyllithium; pyridinium chlorochromate; In dichloromethane;
DOI:10.1039/c1cc10313j

Reference yield:

: 310897-86-0
methyl o-tolylsulfonylcarbamate

: 1309367-83-6
2-(o-tert-butyl phenylsulfonylcarbamate)-1-p-methoxyphenylethanone

Guidance literature:: Multi-step reaction with 2 steps

1: n-butyllithium

2: pyridinium chlorochromate / dichloromethane / 20 °C

With n-butyllithium; pyridinium chlorochromate; In dichloromethane;
DOI:10.1039/c1cc10313j