deoxybenzoin ethylene glycol acetal

Base Information

• Chemical Name: deoxybenzoin ethylene glycol acetal
• CAS No.: 4362-19-0
• Molecular Formula: C₁₆H₁₆O₂
• Molecular Weight: 240.302

Synonyms:deoxybenzoin ethylene glycol acetal

Chemical Property of deoxybenzoin ethylene glycol acetal

Chemical Property:

Purity/Quality:

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Technology Process of deoxybenzoin ethylene glycol acetal

There total 4 articles about deoxybenzoin ethylene glycol acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

2-(2-iodo-1,1-diphenylethoxy)ethanol → deoxybenzoin ethylene glycol acetal (4362-19-0)

Guidance literature:

With Oxone; In ethylene glycol; at 20 ℃; for 2h;

DOI:10.1039/c5ra11092k

Reference yield: 69.0%

ethylene glycol (107-21-1) + diphenyl acetylene (501-65-5) → deoxybenzoin ethylene glycol acetal (4362-19-0)

Guidance literature:

With [{Au(IPr)}2(μ-OH)][BF4]; at 120 ℃; for 72h;

DOI:10.1016/j.jorganchem.2010.08.052

Reference yield:

phenyl benzyl ketone (451-40-1) + ethylene glycol (107-21-1) → deoxybenzoin ethylene glycol acetal (4362-19-0)

Guidance literature:

With toluene-4-sulfonic acid; toluene; Unter Entfernen des entstehenden Wassers_.;

upstream raw materials:

phenyl benzyl ketone

ethylene glycol

diphenyl acetylene

1,1-Diphenylethylene

Downstream raw materials:

benzyl radical

2-Phenyl-1,3-dioxolan-2-ylium carbocation

1-nitro-1-phenylmethane

benzyl nitrate

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