3-[1-Ethylsulfanyl-1-mercapto-meth-(Z)-ylidene]-1-phenyl-indolizin-2-one

Base Information

Chemical Name:3-[1-Ethylsulfanyl-1-mercapto-meth-(Z)-ylidene]-1-phenyl-indolizin-2-one
CAS No.:74360-66-0
Molecular Formula:C₁₇H₁₅NOS₂
Molecular Weight:313.444
Hs Code.:

Synonyms:3-[1-Ethylsulfanyl-1-mercapto-meth-(Z)-ylidene]-1-phenyl-indolizin-2-one

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Chemical Property of 3-[1-Ethylsulfanyl-1-mercapto-meth-(Z)-ylidene]-1-phenyl-indolizin-2-one

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Technology Process of 3-[1-Ethylsulfanyl-1-mercapto-meth-(Z)-ylidene]-1-phenyl-indolizin-2-one

There total 1 articles about 3-[1-Ethylsulfanyl-1-mercapto-meth-(Z)-ylidene]-1-phenyl-indolizin-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

: 75-15-0,12122-00-8
carbon disulfide

: 64-67-5
diethyl sulfate

: 74360-64-8
1-<(ethoxycarbonyl)methyl>-2-benzylpyridinium bromide

: 74360-66-0
3-[1-Ethylsulfanyl-1-mercapto-meth-(Z)-ylidene]-1-phenyl-indolizin-2-one

Guidance literature:: 1-<(ethoxycarbonyl)methyl>-2-benzylpyridinium bromide; With 1,8-diazabicyclo[5.4.0]undec-7-ene; In ethanol; at 60 ℃; for 0.25h;

carbon disulfide; In ethanol; at 20 ℃; for 0.25h;

diethyl sulfate; In ethanol; at 20 ℃; for 1.5h;
DOI:10.3987/COM-10-S(E)72

Reference yield: 91.0%

: 75-03-6
ethyl iodide

: 74360-66-0
3-[1-Ethylsulfanyl-1-mercapto-meth-(Z)-ylidene]-1-phenyl-indolizin-2-one

: 74360-68-2
3-(Bis-ethylsulfanyl-methylene)-1-phenyl-indolizin-2-one

Guidance literature:: With potassium carbonate; In chloroform; for 48h; Ambient temperature;
DOI:10.1246/bcsj.53.1115

Reference yield:

: 74360-66-0
3-[1-Ethylsulfanyl-1-mercapto-meth-(Z)-ylidene]-1-phenyl-indolizin-2-one

: 75159-74-9
3-Acetyl-4-ethylsulfanyl-10-phenyl-pyrano[2,3-b]indolizin-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / K₂CO₃ / CHCl₃ / 48 h / Ambient temperature

2: 84 percent / potassium t-butoxide (KB) / benzene / Heating

With potassium tert-butylate; potassium carbonate; In chloroform; benzene;
DOI:10.1246/bcsj.53.1115