C₄₁H₅₅N₇O₉S

Base Information

Chemical Name:C₄₁H₅₅N₇O₉S
CAS No.:352229-64-2
Molecular Formula:C₄₁H₅₅N₇O₉S
Molecular Weight:821.995
Hs Code.:

C<sub>41</sub>H<sub>55</sub>N<sub>7</sub>O<sub>9</sub>S

Synonyms:C₄₁H₅₅N₇O₉S

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Chemical Property of C₄₁H₅₅N₇O₉S

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Technology Process of C₄₁H₅₅N₇O₉S

There total 4 articles about C₄₁H₅₅N₇O₉S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 189563-95-9
C₄₁H₅₇N₇O₉S

: 352229-64-2
C₄₁H₅₅N₇O₉S

Guidance literature:: With dipyridinium dichromate; 4 A molecular sieve; Celite; In dichloromethane; at 20 ℃; for 3.5h;
DOI:10.1016/S0040-4020(01)00323-4

Reference yield:

: 16874-17-2
L-phenylalanine tert-butyl ester

: 352229-64-2
C₄₁H₅₅N₇O₉S

Guidance literature:: Multi-step reaction with 6 steps

1.1: 85.9 percent / acetonitrile / 2.5 h / 20 °C

2.1: N-methylmorpholine / CH₂Cl₂

2.2: 70 percent / CH₂Cl₂ / 24 h / 20 °C

3.1: 99 percent / H₂ / Pd/C / acetic acid / 2.5 h / 20 °C

4.1: N-methylmorpholine / tetrahydrofuran / 0 °C

4.2: 90 percent / EDCI; HOBt / CH₂Cl₂ / 0 - 20 °C

5.1: 92 percent / H₂ / Pd/C / acetic acid / 4.5 h / 20 °C

6.1: 63 percent / PDC; 4 Angstroem molecular sieves; celite 545 / CH₂Cl₂ / 3.5 h / 20 °C

With 4-methyl-morpholine; dipyridinium dichromate; 4 A molecular sieve; Celite; hydrogen; palladium on activated charcoal; In tetrahydrofuran; dichloromethane; acetic acid; acetonitrile;
DOI:10.1016/S0040-4020(01)00323-4

Reference yield:

: 189563-82-4
L-phenylalanine t-butyl ester N-hydroxysuccinimide carboxamide

: 352229-64-2
C₄₁H₅₅N₇O₉S

Guidance literature:: Multi-step reaction with 5 steps

1.1: N-methylmorpholine / CH₂Cl₂

1.2: 70 percent / CH₂Cl₂ / 24 h / 20 °C

2.1: 99 percent / H₂ / Pd/C / acetic acid / 2.5 h / 20 °C

3.1: N-methylmorpholine / tetrahydrofuran / 0 °C

3.2: 90 percent / EDCI; HOBt / CH₂Cl₂ / 0 - 20 °C

4.1: 92 percent / H₂ / Pd/C / acetic acid / 4.5 h / 20 °C

5.1: 63 percent / PDC; 4 Angstroem molecular sieves; celite 545 / CH₂Cl₂ / 3.5 h / 20 °C

With 4-methyl-morpholine; dipyridinium dichromate; 4 A molecular sieve; Celite; hydrogen; palladium on activated charcoal; In tetrahydrofuran; dichloromethane; acetic acid;
DOI:10.1016/S0040-4020(01)00323-4