Technology Process of C55H87N7O22
There total 12 articles about C55H87N7O22 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
pyridine;
In
dichloromethane;
at 0 - 20 ℃;
for 20h;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: sodium hydrogencarbonate / water; acetone / 18 h
2: N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline / methanol; dichloromethane / 20 °C
3: diethylamine / dichloromethane; acetonitrile / 17 h / 0 - 20 °C
4: HATU; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 2 h / 20 °C
5: HATU; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 2 h / 20 °C
6: pyridine / dichloromethane / 20 h / 0 - 20 °C
With
pyridine; sodium hydrogencarbonate; N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline; diethylamine; N-ethyl-N,N-diisopropylamine; HATU;
In
tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; acetone; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: tetrabutylammonium hydrogen sulfate; potassium hydroxide / toluene / 5 h / 0 - 20 °C
2: trifluoroacetic acid / dichloromethane / 2 h / 20 °C
3: HATU; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 2 h / 20 °C
4: HATU; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 2 h / 20 °C
5: pyridine / dichloromethane / 20 h / 0 - 20 °C
With
pyridine; tetrabutylammonium hydrogen sulfate; N-ethyl-N,N-diisopropylamine; HATU; trifluoroacetic acid; potassium hydroxide;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; toluene;