Technology Process of β-Anilinochalcon-anil
There total 6 articles about β-Anilinochalcon-anil which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
aluminium trichloride;
In
1,4-dioxane;
at 100 ℃;
for 72h;
DOI:10.1055/s-1986-31676
- Guidance literature:
-
phenyl(1-phenylethylidene)amine;
With
lithium diisopropyl amide;
In
tetrahydrofuran; hexane;
at -10 ℃;
for 0.5h;
Inert atmosphere;
N-phenyl-benzimidoyl chloride;
In
tetrahydrofuran; hexane;
at -10 - 20 ℃;
for 12h;
Inert atmosphere;
DOI:10.1021/ja510985v
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: 24 h / 20 °C / Molecular sieve; Inert atmosphere
2.1: lithium diisopropyl amide / hexane; tetrahydrofuran / 0.5 h / -10 °C / Inert atmosphere
2.2: 12 h / -10 - 20 °C / Inert atmosphere
With
lithium diisopropyl amide;
In
tetrahydrofuran; hexane;
DOI:10.1021/ja510985v
