methyl 4-ethynylphenylcarbamate

Base Information

Chemical Name:methyl 4-ethynylphenylcarbamate
CAS No.:1404481-77-1
Molecular Formula:C₁₀H₉NO₂
Molecular Weight:175.187
Hs Code.:

Synonyms:methyl 4-ethynylphenylcarbamate

Suppliers and Price of methyl 4-ethynylphenylcarbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of methyl 4-ethynylphenylcarbamate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of methyl 4-ethynylphenylcarbamate

There total 3 articles about methyl 4-ethynylphenylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1370470-71-5
1,3,5-tris{4-[(trimethylsilyl)ethynyl]phenyl}-1,3,5-triazinane-2,4,6-trione

: 1404481-77-1
methyl 4-ethynylphenylcarbamate

Guidance literature:: With potassium carbonate; In tetrahydrofuran; methanol; at 20 ℃; for 4h; Inert atmosphere;
DOI:10.1002/chem.201200484

Reference yield: 78.0%

: 681-84-5
tetramethylorthosilicate

: 124-38-9,18923-20-1
carbon dioxide

: 14235-81-5
4-Ethynylaniline

: 1404481-77-1
methyl 4-ethynylphenylcarbamate

Guidance literature:: With 2,3,4,5,7,8,9,10-octahydropyrimido[1,2-a]azepin-1-ium acetate; In acetonitrile; at 150 ℃; for 24h; under 37503.8 Torr; chemoselective reaction; Autoclave; Inert atmosphere; Ionic liquid; Green chemistry;
DOI:10.1039/c7gc02666h

Reference yield: 65.0%

: 67-56-1
methanol

: 124-38-9,18923-20-1
carbon dioxide

: 14235-81-5
4-Ethynylaniline

: 1404481-77-1
methyl 4-ethynylphenylcarbamate

Guidance literature:: With calcium carbide; potassium carbonate; In acetonitrile; at 180 ℃; for 24h; under 37503.8 Torr; Autoclave; Glovebox; Sealed tube;
DOI:10.1039/d0gc01402h