(2S)-2-{methoxymethyl[2-(2,2,2-trifluoroacetylamino)acetyl]amino}-3-phenylpropionic acid methyl ester

Base Information

Chemical Name:(2S)-2-{methoxymethyl[2-(2,2,2-trifluoroacetylamino)acetyl]amino}-3-phenylpropionic acid methyl ester
CAS No.:429685-01-8
Molecular Formula:C₁₆H₁₉F₃N₂O₅
Molecular Weight:376.332
Hs Code.:

Synonyms:(2S)-2-{methoxymethyl[2-(2,2,2-trifluoroacetylamino)acetyl]amino}-3-phenylpropionic acid methyl ester

Suppliers and Price of (2S)-2-{methoxymethyl[2-(2,2,2-trifluoroacetylamino)acetyl]amino}-3-phenylpropionic acid methyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (2S)-2-{methoxymethyl[2-(2,2,2-trifluoroacetylamino)acetyl]amino}-3-phenylpropionic acid methyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (2S)-2-{methoxymethyl[2-(2,2,2-trifluoroacetylamino)acetyl]amino}-3-phenylpropionic acid methyl ester

There total 3 articles about (2S)-2-{methoxymethyl[2-(2,2,2-trifluoroacetylamino)acetyl]amino}-3-phenylpropionic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 67-56-1
methanol

: 429685-00-7
3-phenyl-2-{[2-(2,2,2-trifluoroacetylamino)acetyl]trimethylsilylmethylamino}propionic acid methyl ester

: 429685-01-8
(2S)-2-{methoxymethyl[2-(2,2,2-trifluoroacetylamino)acetyl]amino}-3-phenylpropionic acid methyl ester

Guidance literature:: With tetrabutylammonium tetrafluoroborate; Electrolysis;
DOI:10.1021/ja064737l

Reference yield:

: 220438-32-4
(S)-(+)-methyl 2-<(trimethylsilyl)methyl>amino-3-phenylpropionate

: 429685-01-8
(2S)-2-{methoxymethyl[2-(2,2,2-trifluoroacetylamino)acetyl]amino}-3-phenylpropionic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 243 mg / triethylamine / diethyl ether / 12 h / 20 °C

2: 70 percent / tetrabutylammonium tetrafluoroborate / Electrolysis

With tetrabutylammonium tetrafluoroborate; triethylamine; In diethyl ether;
DOI:10.1021/ja064737l

Reference yield:

: 7524-50-7
methyl (2S)-2-amino-3-phenylpropanoate hydrochloride

: 429685-01-8
(2S)-2-{methoxymethyl[2-(2,2,2-trifluoroacetylamino)acetyl]amino}-3-phenylpropionic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 69 percent / potassium iodide; potassium carbonate / dimethylformamide / 12 h / 90 °C

2: 243 mg / triethylamine / diethyl ether / 12 h / 20 °C

3: 70 percent / tetrabutylammonium tetrafluoroborate / Electrolysis

With tetrabutylammonium tetrafluoroborate; potassium carbonate; triethylamine; potassium iodide; In diethyl ether; N,N-dimethyl-formamide;
DOI:10.1021/ja064737l