2--2-trimethylsilyl-1,3-dithiane ammonium triflate salt

Base Information

Chemical Name:2--2-trimethylsilyl-1,3-dithiane ammonium triflate salt
CAS No.:101681-24-7
Molecular Formula:CF₃O₃S*C₁₇H₃₀NS₂Si
Molecular Weight:489.72
Hs Code.:

2-<o-(N,N-Dimethylaminomethyl)-phenyl>-2-trimethylsilyl-1,3-dithiane ammonium triflate salt

Synonyms:2--2-trimethylsilyl-1,3-dithiane ammonium triflate salt

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Chemical Property of 2--2-trimethylsilyl-1,3-dithiane ammonium triflate salt

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Technology Process of 2--2-trimethylsilyl-1,3-dithiane ammonium triflate salt

There total 3 articles about 2--2-trimethylsilyl-1,3-dithiane ammonium triflate salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 101681-22-5
2--2-trimethylsilyl-1,3-dithiane

: 333-27-7
methyl trifluoromethanesulfonate

: 101681-24-7
2--2-trimethylsilyl-1,3-dithiane ammonium triflate salt

Guidance literature:: In dichloromethane; at 0 ℃; for 4h;

Reference yield:

: 19886-78-3
1-formyl-2-[(dimethylamino)methyl]benzene

: 101681-24-7
2--2-trimethylsilyl-1,3-dithiane ammonium triflate salt

Guidance literature:: Multi-step reaction with 3 steps

1: 50 percent / boron trifluoride etherate

2: 1.) n-BuLi / THF, hexane, 1.) -30 deg C, 3 h, 2.) -78 deg C to room temp., overnight

3: 100 percent / CH₂Cl₂ / 4 h / 0 °C

With n-butyllithium; boron trifluoride diethyl etherate; In dichloromethane;

Reference yield:

: 101707-70-4
2--1,3-dithiane

: 101681-24-7
2--2-trimethylsilyl-1,3-dithiane ammonium triflate salt

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) n-BuLi / THF, hexane, 1.) -30 deg C, 3 h, 2.) -78 deg C to room temp., overnight

2: 100 percent / CH₂Cl₂ / 4 h / 0 °C

With n-butyllithium; In dichloromethane;