11-[2-allyloxy-3-(4,5-dihydro-1,3-dioxol-2-yl)phenoxy]-3,6,9-trioxaundecylamine

Base Information

Chemical Name:11-[2-allyloxy-3-(4,5-dihydro-1,3-dioxol-2-yl)phenoxy]-3,6,9-trioxaundecylamine
CAS No.:382162-15-4
Molecular Formula:C₂₀H₃₁NO₇
Molecular Weight:397.469
Hs Code.:

Synonyms:11-[2-allyloxy-3-(4,5-dihydro-1,3-dioxol-2-yl)phenoxy]-3,6,9-trioxaundecylamine

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Chemical Property of 11-[2-allyloxy-3-(4,5-dihydro-1,3-dioxol-2-yl)phenoxy]-3,6,9-trioxaundecylamine

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Technology Process of 11-[2-allyloxy-3-(4,5-dihydro-1,3-dioxol-2-yl)phenoxy]-3,6,9-trioxaundecylamine

There total 8 articles about 11-[2-allyloxy-3-(4,5-dihydro-1,3-dioxol-2-yl)phenoxy]-3,6,9-trioxaundecylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 382162-14-3
N-[11-(2-allyloxy-3-(4,5-dihydro-1,3-dioxol-2-yl)phenoxy)-3,6,9-trioxaundecyl]phthalimide

: 382162-15-4
11-[2-allyloxy-3-(4,5-dihydro-1,3-dioxol-2-yl)phenoxy]-3,6,9-trioxaundecylamine

Guidance literature:: With hydrazine hydrate; In methanol; for 5h; Heating;
DOI:10.1039/b103274g

Reference yield:

: 112-60-7
Tetraethylene glycol

: 382162-15-4
11-[2-allyloxy-3-(4,5-dihydro-1,3-dioxol-2-yl)phenoxy]-3,6,9-trioxaundecylamine

Guidance literature:: Multi-step reaction with 6 steps

1: 28 g / triethylamine; DMAP / CH₂Cl₂ / 10 h / 20 °C

2: 84 percent / dimethylformamide / 8 h / 100 °C

3: 64 percent / triethylamine; DMAP / CH₂Cl₂ / 6 h / 20 °C

4: 83 percent / K₂CO₃ / acetonitrile / 48 h / Heating

5: 100 percent / trimethyl orthoformate; toluene-p-sulfonic acid / toluene / 8 h / Heating

6: 79 percent / N₂H₄*H₂O / methanol / 5 h / Heating

With dmap; potassium carbonate; toluene-4-sulfonic acid; hydrazine hydrate; triethylamine; trimethyl orthoformate; In methanol; dichloromethane; N,N-dimethyl-formamide; toluene; acetonitrile;
DOI:10.1039/b103274g

Reference yield:

: 24677-78-9
2,3-dihydroxybenzaldehyde

: 382162-15-4
11-[2-allyloxy-3-(4,5-dihydro-1,3-dioxol-2-yl)phenoxy]-3,6,9-trioxaundecylamine

Guidance literature:: Multi-step reaction with 4 steps

1: 50 percent / NaH / dimethylsulfoxide / 20 °C

2: 83 percent / K₂CO₃ / acetonitrile / 48 h / Heating

3: 100 percent / trimethyl orthoformate; toluene-p-sulfonic acid / toluene / 8 h / Heating

4: 79 percent / N₂H₄*H₂O / methanol / 5 h / Heating

With sodium hydride; potassium carbonate; toluene-4-sulfonic acid; hydrazine hydrate; trimethyl orthoformate; In methanol; dimethyl sulfoxide; toluene; acetonitrile;
DOI:10.1039/b103274g