N-[11-(2-allyloxy-3-(4,5-dihydro-1,3-dioxol-2-yl)phenoxy)-3,6,9-trioxaundecyl]phthalimide

Base Information

Chemical Name:N-[11-(2-allyloxy-3-(4,5-dihydro-1,3-dioxol-2-yl)phenoxy)-3,6,9-trioxaundecyl]phthalimide
CAS No.:382162-14-3
Molecular Formula:C₂₈H₃₃NO₉
Molecular Weight:527.571
Hs Code.:

Synonyms:N-[11-(2-allyloxy-3-(4,5-dihydro-1,3-dioxol-2-yl)phenoxy)-3,6,9-trioxaundecyl]phthalimide

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Chemical Property of N-[11-(2-allyloxy-3-(4,5-dihydro-1,3-dioxol-2-yl)phenoxy)-3,6,9-trioxaundecyl]phthalimide

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Technology Process of N-[11-(2-allyloxy-3-(4,5-dihydro-1,3-dioxol-2-yl)phenoxy)-3,6,9-trioxaundecyl]phthalimide

There total 7 articles about N-[11-(2-allyloxy-3-(4,5-dihydro-1,3-dioxol-2-yl)phenoxy)-3,6,9-trioxaundecyl]phthalimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 107-21-1
ethylene glycol

: 382162-13-2
N-[11-(2-allyloxy-3-formylphenoxy)-3,6,9-trioxaundecyl]phthalimide

: 382162-14-3
N-[11-(2-allyloxy-3-(4,5-dihydro-1,3-dioxol-2-yl)phenoxy)-3,6,9-trioxaundecyl]phthalimide

Guidance literature:: With toluene-4-sulfonic acid; trimethyl orthoformate; In toluene; for 8h; Heating;
DOI:10.1039/b103274g

Reference yield:

: 112-60-7
Tetraethylene glycol

: 382162-14-3
N-[11-(2-allyloxy-3-(4,5-dihydro-1,3-dioxol-2-yl)phenoxy)-3,6,9-trioxaundecyl]phthalimide

Guidance literature:: Multi-step reaction with 5 steps

1: 28 g / triethylamine; DMAP / CH₂Cl₂ / 10 h / 20 °C

2: 84 percent / dimethylformamide / 8 h / 100 °C

3: 64 percent / triethylamine; DMAP / CH₂Cl₂ / 6 h / 20 °C

4: 83 percent / K₂CO₃ / acetonitrile / 48 h / Heating

5: 100 percent / trimethyl orthoformate; toluene-p-sulfonic acid / toluene / 8 h / Heating

With dmap; potassium carbonate; toluene-4-sulfonic acid; triethylamine; trimethyl orthoformate; In dichloromethane; N,N-dimethyl-formamide; toluene; acetonitrile;
DOI:10.1039/b103274g

Reference yield:

: 24677-78-9
2,3-dihydroxybenzaldehyde

: 382162-14-3
N-[11-(2-allyloxy-3-(4,5-dihydro-1,3-dioxol-2-yl)phenoxy)-3,6,9-trioxaundecyl]phthalimide

Guidance literature:: Multi-step reaction with 3 steps

1: 50 percent / NaH / dimethylsulfoxide / 20 °C

2: 83 percent / K₂CO₃ / acetonitrile / 48 h / Heating

3: 100 percent / trimethyl orthoformate; toluene-p-sulfonic acid / toluene / 8 h / Heating

With sodium hydride; potassium carbonate; toluene-4-sulfonic acid; trimethyl orthoformate; In dimethyl sulfoxide; toluene; acetonitrile;
DOI:10.1039/b103274g