(-)-(1S,2S)-2-(3-hydroxypropyl)-1,3,3-trimethylcyclohexanecarboxylate

Base Information

Chemical Name:(-)-(1S,2S)-2-(3-hydroxypropyl)-1,3,3-trimethylcyclohexanecarboxylate
CAS No.:97855-68-0
Molecular Formula:C₁₄H₂₆O₃
Molecular Weight:242.359
Hs Code.:

Synonyms:(-)-(1S,2S)-2-(3-hydroxypropyl)-1,3,3-trimethylcyclohexanecarboxylate

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Chemical Property of (-)-(1S,2S)-2-(3-hydroxypropyl)-1,3,3-trimethylcyclohexanecarboxylate

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Technology Process of (-)-(1S,2S)-2-(3-hydroxypropyl)-1,3,3-trimethylcyclohexanecarboxylate

There total 7 articles about (-)-(1S,2S)-2-(3-hydroxypropyl)-1,3,3-trimethylcyclohexanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 110715-80-5
(-)-(1S,8aS)-1,2,3,5,6,7,8,8a-octahydro-5,5,8a-trimethylnaphthalen-1-ol

: 97855-68-0
(-)-(1S,2S)-2-(3-hydroxypropyl)-1,3,3-trimethylcyclohexanecarboxylate

Guidance literature:: Multi-step reaction with 6 steps

1: 95 percent / H₂ / Adam's catalyst / acetic acid

2: 90 percent / Florisil, PCC / CH₂Cl₂ / 2 h / Ambient temperature

3: 97 percent / PBB / acetic acid / 2 h / Ambient temperature

4: 97 percent / sodium hydroxide / dimethylformamide; H₂O / 0.5 h / Ambient temperature

5: lead tetra-acetate (LTA) / benzene / 0.17 h / Ambient temperature

6: NaBH₄ / methanol / 0.33 h / Ambient temperature

With lead(IV) acetate; sodium hydroxide; sodium tetrahydroborate; florisil; hydrogen; pyridinium chlorochromate; platinum(IV) oxide; In methanol; dichloromethane; water; acetic acid; N,N-dimethyl-formamide; benzene;

Reference yield:

: 110654-75-6
(+)-(4aS,5S)-5-benzoyloxy-3,4,4a,5,6,7-hexahydro-1,1,4a-trimethylnaphthalen-2(1H)-one

: 97855-68-0
(-)-(1S,2S)-2-(3-hydroxypropyl)-1,3,3-trimethylcyclohexanecarboxylate

Guidance literature:: Multi-step reaction with 7 steps

1: 93 percent / potassium hydroxide, hydrazine hydrate / bis-(2-hydroxy-ethyl) ether / 6 h / Heating

2: 95 percent / H₂ / Adam's catalyst / acetic acid

3: 90 percent / Florisil, PCC / CH₂Cl₂ / 2 h / Ambient temperature

4: 97 percent / PBB / acetic acid / 2 h / Ambient temperature

5: 97 percent / sodium hydroxide / dimethylformamide; H₂O / 0.5 h / Ambient temperature

6: lead tetra-acetate (LTA) / benzene / 0.17 h / Ambient temperature

7: NaBH₄ / methanol / 0.33 h / Ambient temperature

With lead(IV) acetate; potassium hydroxide; sodium hydroxide; sodium tetrahydroborate; florisil; hydrogen; hydrazine hydrate; pyridinium chlorochromate; platinum(IV) oxide; In methanol; dichloromethane; water; acetic acid; N,N-dimethyl-formamide; diethylene glycol; benzene;